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三氟-1-9-蒽乙醇

产品名称 三氟-1-9-蒽乙醇

CAS号60646-30-2

分子式C16H11F3O

分子量276.25


  • Mass

    MS-IW-0785          
    (S)-(+)-1-(9-anthryl)-2,2,2-trifluoroethanol
    C16H11F3O           (Mass of molecular ion:    276)
    

       Source Temperature: 120 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          18.0       1.1
          63.0       1.1
          75.0       1.9
          76.0       4.8
          88.0       5.9
          88.5       2.3
          89.0       7.4
          89.5       1.8
         103.5       7.8
         104.0       1.4
         138.0       1.4
         150.0       1.5
         151.0       2.5
         152.0       1.9
         176.0       6.6
         177.0       6.7
         178.0      32.4
         179.0      42.5
         180.0       6.1
         205.0       1.9
         206.0       1.6
         207.0      69.2
         208.0      11.5
         209.0       1.3
         239.0       1.3
         275.0       2.5
         276.0     100.0
         277.0      17.5
         278.0       1.7
    

400 MHz (at 40.C)


  • 1H NMR 399.65 MHz
    C16 H11 F3 O 0.037 g : 0.5 ml CDCl3 at 40C
    (S)-(+)-1-(9-anthryl)-2,2,2-trifluoroethanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 8.9 B 8.464 C *1 8.2 D 7.972 E *2 7.514 F *2 7.445 G 6.574 J 2.90 J(G,J)=4.4HZ J(F-19,G)=8.1HZ

         Hz     ppm     Int.
    

       3382.87   8.465   1000
       3190.46   7.984    787
       3182.07   7.963    855
       3012.24   7.538    452
       3010.71   7.534    488
       3005.68   7.521    740
       3004.15   7.517    747
       3003.23   7.515    522
       3001.56   7.511    467
       2996.52   7.498    728
       2995.15   7.495    675
       2991.64   7.486     39
       2982.79   7.464    812
       2981.72   7.461    844
       2976.23   7.448    548
       2974.55   7.443    843
       2973.48   7.441    785
       2967.83   7.427    508
       2966.92   7.424    496
       2642.06   6.611     94
       2637.63   6.600    102
       2633.97   6.591    288
       2629.70   6.581    297
       2626.04   6.571    301
       2621.61   6.560    301
       2617.95   6.551    110
       2613.68   6.540    103
       1160.43   2.904    890
       1156.01   2.893    868
    

in CDCl3



KBr disc



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