-
MassMS-NW-2566 9,10-dichloroanthracene C14H8Cl2 (Mass of molecular ion: 246)
Source Temperature: 200 °C Sample Temperature: 130 °C Direct, 75 eV
18.0 1.5 36.0 1.3 39.0 1.2 50.0 1.9 51.0 1.6 61.0 1.9 62.0 2.7 63.0 2.2 73.0 1.4 74.0 6.1 75.0 6.4 76.0 1.2 85.0 1.6 86.0 2.7 87.0 11.2 88.0 12.5 92.0 1.5 93.0 1.9 98.0 4.3 99.0 3.1 100.0 1.0 105.0 6.5 106.0 2.1 110.0 4.8 111.0 3.2 122.0 2.1 123.0 13.1 124.0 7.7 125.0 1.9 126.0 1.5 149.0 4.8 150.0 7.8 151.0 1.3 173.0 1.3 174.0 15.0 175.0 18.2 176.0 79.0 177.0 11.6 210.0 8.4 211.0 8.6 212.0 4.0 213.0 2.8 246.0 100.0 247.0 15.4 248.0 62.0 249.0 9.3 250.0 10.5 251.0 1.4
parameter in CDCl3
-
1H NMR 300 MHz C14 H8 Cl2 in CDCl3 9,10-dichloroanthracene 
Parameter ppm Hz
D(A) 8.55 D(B) 7.64 J(A,A') 0.5 J(A,B) 8.9 J(A,B') 1.1 J(A',B) 1.1 J(A',B') 8.9 J(B,B') 8.0 SHARPLESS,N.E. ET AL. ORG.MAGN.RESON. 6, 115 (1974)
Hz ppm Int.2575.08 8.584 77 2574.23 8.581 88 2570.08 8.567 931 2566.66 8.556 814 2563.49 8.545 807 2560.08 8.534 1000 2555.88 8.520 102 2555.11 8.517 90 2301.90 7.673 90 2301.13 7.670 102 2296.93 7.656 1000 2293.52 7.645 807 2290.35 7.634 814 2286.93 7.623 931 2282.78 7.609 88 2281.93 7.606 77
CCl4 solution
KBr disc
nujol mull
更多供应商
