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网站主页CAS数据库列表 6033-32-5更多图谱L-6-羟基正亮氨酸(6033-32-5)核磁图(13CNMR)

L-6-羟基正亮氨酸

产品名称 L-6-羟基正亮氨酸

CAS号6033-32-5

分子式C6H13NO3

分子量147.17

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  • Mass

    MS-IW-9682          
    6-hydroxy-L-norleucine
    C6H13NO3            (Mass of molecular ion:    147)
    

       Source Temperature: 190 °C
       Sample Temperature: 200 °C
       Direct, 75 eV
    

          15.0       3.8
          16.0       1.3
          17.0      11.0
          18.0      53.1
          19.0       1.0
          25.0       1.4
          26.0      11.4
          27.0      27.7
          28.0      87.3
          29.0      21.5
          30.0      26.9
          31.0      10.0
          37.0       1.7
          38.0       3.5
          39.0      18.6
          40.0       6.4
          41.0      37.1
          42.0      24.2
          43.0      68.5
          44.0      11.2
          45.0       2.4
          46.0       6.7
          50.0       3.6
          51.0       5.4
          52.0       8.5
          53.0       8.0
          54.0      15.4
          55.0      29.8
          56.0     100.0
          57.0      24.6
          58.0       1.5
          63.0       1.1
          64.0       1.3
          65.0       3.7
          66.0       6.7
          67.0      16.9
          68.0       4.6
          69.0       3.8
          70.0       2.9
          71.0       4.3
          72.0       2.9
          73.0       1.7
          74.0      21.7
          75.0       3.9
          78.0       2.3
          79.0       5.3
          80.0       3.8
          81.0       2.9
          82.0      11.1
          83.0      10.8
          84.0      30.0
          85.0      39.1
          86.0       2.6
          87.0       1.5
          91.0       1.5
          92.0       1.6
          93.0       7.4
          94.0       1.9
         100.0       1.5
         101.0       1.8
         102.0      27.8
         103.0       1.8
         111.0       1.6
         129.0       1.4
    

400 MHz in D2O


  • 1H NMR 399.65 MHz
    C6 H13 N O3 0.035 g : 0.5 ml D2O
    6-hydroxy-L-norleucine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.746 B 3.624 C 1.89 D 1.603 E 1.45 THE SOLVENT PEAK SUPPRESSED.

         Hz     ppm     Int.
    

       1503.30   3.762    194
       1497.07   3.746    313
       1490.97   3.731    188
       1454.83   3.641    504
       1448.49   3.625   1000
       1441.89   3.608    491
        764.04   1.912    168
        762.57   1.909    172
        762.33   1.908    172
        758.79   1.899    175
        755.00   1.890    219
        753.66   1.886    222
        748.05   1.872    195
        746.70   1.869    176
        746.22   1.868    177
        648.32   1.623    288
        641.36   1.605    482
        634.40   1.588    404
        627.69   1.571    152
        586.67   1.468    151
        584.23   1.462    143
        577.51   1.446    220
        573.12   1.435    138
        570.19   1.427    191
    

in D2O



KBr disc



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