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网站主页CAS数据库列表 602-56-2更多图谱9-苯基吖啶(602-56-2)核磁图(1HNMR)

9-苯基吖啶

产品名称 9-苯基吖啶

CAS号602-56-2

分子式C19H13N

分子量255.31

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  • Mass

    MS-IW-7578          
    9-phenylacridine
    C19H13N             (Mass of molecular ion:    255)
    

       Source Temperature: 160 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

         100.0       2.9
         100.5       1.0
         101.0       1.2
         112.0       2.8
         112.5       2.0
         113.0       4.9
         113.5       2.2
         114.0       3.8
         125.5       1.5
         126.0      10.6
         126.5       7.3
         127.0      13.7
         127.5       9.8
         128.0       1.9
         200.0       1.3
         201.0       1.2
         202.0       1.2
         224.0       1.3
         225.0       2.2
         226.0       5.2
         227.0       3.4
         228.0       1.4
         240.0       1.1
         251.0       4.3
         252.0       7.0
         253.0      12.6
         254.0      64.3
         255.0     100.0
         256.0      19.5
         257.0       1.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C19 H13 N 0.040 g : 0.5 ml CDCl3
    9-phenylacridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.280 B 7.747 C 7.691 D 7.57 E 7.42 F 7.395 J(A,B)=8.8HZ J(A,F)=1.1HZ J(A,C)=0.7HZ J(B,C)=1.4HZ J(B,F)=6.6HZ J(C,F)=8.8HZ ASSIGNED BY C-H COSY

         Hz     ppm     Int.
    

       3314.58   8.294    427
       3313.84   8.292    564
       3313.48   8.291    568
       3312.74   8.290    468
       3309.20   8.281     37
       3305.79   8.272    478
       3305.05   8.270    634
       3303.96   8.268    513
       3104.86   7.769    331
       3103.39   7.766    382
       3100.83   7.759     48
       3098.27   7.753    392
       3096.80   7.749    454
       3096.07   7.747    388
       3094.60   7.744    383
       3089.48   7.731    351
       3088.13   7.728    398
       3084.47   7.718     30
       3079.71   7.707    420
       3079.10   7.705    492
       3078.37   7.703    481
       3077.76   7.702    409
       3070.92   7.685    496
       3070.31   7.683    592
       3069.58   7.681    545
       3068.97   7.680    466
       3063.48   7.666     44
       3054.57   7.644     35
       3039.18   7.605     86
       3037.48   7.601     65
       3035.77   7.597    133
       3034.30   7.593     93
       3033.08   7.590     93
       3030.64   7.584    417
       3030.15   7.583    416
       3028.56   7.579    288
       3026.61   7.574    213
       3025.15   7.570    393
       3023.19   7.565   1000
       3021.48   7.561    377
       3020.51   7.558    251
       3017.82   7.552    201
       3016.48   7.548    158
       3011.47   7.536     61
       3009.77   7.532     54
       2969.60   7.431    544
       2967.53   7.426    413
       2967.04   7.425    395
       2965.45   7.421    223
       2963.50   7.416    613
       2962.28   7.413    692
       2960.21   7.408    478
       2957.15   7.400    439
       2955.93   7.397    443
       2954.83   7.394    429
       2953.61   7.391    411
       2950.44   7.383     53
       2948.36   7.378    344
       2947.14   7.375    348
    

in CDCl3



KBr disc



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