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MassMS-NW-5840 di-sec-butyl disulfide C8H18S2 (Mass of molecular ion: 178)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 6.1 28.0 1.5 29.0 22.4 39.0 4.6 41.0 24.5 42.0 1.3 45.0 1.7 47.0 1.1 53.0 1.2 55.0 4.7 56.0 6.4 57.0 100.0 58.0 4.2 59.0 3.0 60.0 1.0 61.0 2.6 66.0 1.4 87.0 1.0 88.0 1.4 90.0 1.0 93.0 1.3 122.0 26.9 123.0 1.8 124.0 2.5 178.0 17.9 179.0 2.1 180.0 1.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H18 S2 0.04 ml : 0.5 ml CDCl3 di-sec-butyl disulfide 
Assign. Shift(ppm)
A 2.728 B 1.60 C 1.289 D 0.987
Hz ppm Int.254.63 2.844 46 248.00 2.770 84 241.50 2.697 99 234.88 2.623 62 163.44 1.825 30 156.88 1.752 32 155.50 1.737 88 154.81 1.729 41 149.38 1.668 90 147.81 1.651 125 147.31 1.645 95 141.63 1.582 124 140.31 1.567 154 134.75 1.505 72 133.31 1.489 101 126.94 1.418 48 126.44 1.412 42 118.69 1.326 1000 116.50 1.301 35 111.94 1.250 869 109.75 1.226 34 94.50 1.056 303 92.25 1.031 64 87.19 0.974 482 80.81 0.903 100 80.00 0.894 170 78.81 0.880 102
in CDCl3
liquid film
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