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MS-NW-4936 2-chloro-2-methylbutane C5H11Cl (Mass of molecular ion: 106)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 3.9 18.0 1.2 26.0 3.5 27.0 27.8 28.0 2.6 29.0 32.4 35.0 1.0 36.0 7.9 37.0 1.4 38.0 2.8 39.0 28.2 40.0 4.2 41.0 84.9 42.0 18.1 43.0 84.4 44.0 3.3 49.0 2.3 50.0 1.9 51.0 2.7 52.0 1.0 53.0 7.5 54.0 1.8 55.0 89.5 56.0 5.7 61.0 1.0 63.0 7.1 65.0 2.4 67.0 1.0 69.0 3.0 70.0 20.5 71.0 95.2 72.0 5.4 76.0 60.2 77.0 100.0 78.0 22.9 79.0 33.8 80.0 1.2 90.0 1.6 91.0 18.5 92.0 1.3 93.0 5.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H11 Cl 0.04 ml : 0.5 ml CDCl3 2-chloro-2-methylbutane Assign. Shift(ppm)
A 1.764 B 1.556 C 1.036
Hz ppm Int.
163.25 1.823 53 157.13 1.755 32 155.88 1.741 77 149.50 1.670 29 148.50 1.659 29 141.31 1.578 24 139.44 1.557 1000 137.44 1.535 52 100.06 1.118 51 99.38 1.110 95 98.69 1.102 59 92.44 1.033 245 91.75 1.025 101 85.56 0.956 37 84.75 0.947 61 83.81 0.936 34
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