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MassMS-NW-8076 6-hydroxy-8-methyl-8-azabicyclo(3.2.1)octan-3-one C8H13NO2 (Mass of molecular ion: 155)
Source Temperature: 140 °C Sample Temperature: 110 °C Direct, 75 eV
15.0 7.4 18.0 2.2 26.0 1.1 27.0 7.5 28.0 10.8 29.0 5.2 30.0 3.8 31.0 2.0 39.0 6.0 40.0 1.5 41.0 15.9 42.0 77.0 43.0 7.4 44.0 5.9 53.0 2.5 54.0 5.5 55.0 12.7 56.0 9.0 57.0 16.4 58.0 9.7 67.0 2.3 68.0 5.0 69.0 5.5 70.0 6.5 71.0 2.0 72.0 3.2 80.0 1.7 81.0 2.7 82.0 39.9 83.0 85.3 84.0 9.6 86.0 1.3 94.0 7.2 95.0 1.5 96.0 12.7 97.0 21.7 98.0 17.3 99.0 1.2 110.0 11.9 111.0 100.0 112.0 18.3 113.0 2.0 126.0 3.7 138.0 3.3 155.0 45.3 156.0 5.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H13 N O2 0.030 g : 0.5 ml CDCl3 6-hydroxy-8-methyl-8-azabicyclo(3.2.1)octan-3-one 
Assign. Shift(ppm)
A 4.067 B 3.597 C 3.383 D 3.1 E 2.68 F 2.655 G *1 2.206 J *1 2.095 K 2.055 L 1.994 ASSIGNED BY C-H COSY
Hz ppm Int.1630.49 4.080 69 1627.93 4.074 74 1623.54 4.063 74 1620.85 4.056 71 1441.53 3.607 34 1437.99 3.599 45 1436.65 3.595 47 1435.06 3.591 38 1432.62 3.585 36 1431.27 3.582 32 1354.74 3.390 68 1349.61 3.377 70 1085.33 2.716 38 1080.69 2.705 85 1075.32 2.691 56 1071.17 2.681 38 1069.21 2.676 43 1064.33 2.664 116 1061.04 2.655 1000 891.24 2.231 47 889.40 2.226 82 887.57 2.221 49 874.88 2.190 38 873.17 2.185 70 871.34 2.181 42 848.02 2.122 48 846.07 2.118 79 844.12 2.113 42 836.18 2.093 31 832.28 2.083 45 830.20 2.078 88 828.25 2.073 57 821.90 2.057 73 814.82 2.039 70 805.42 2.016 49 803.34 2.011 31 798.34 1.998 46
in CDCl3
KBr disc
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