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MassMS-NW-6414 (chloromethyl)cyclopropane C4H7Cl (Mass of molecular ion: 90)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.0 26.0 6.9 27.0 32.2 28.0 8.6 29.0 22.0 36.0 1.4 37.0 1.8 38.0 3.1 39.0 27.7 40.0 2.2 41.0 27.8 42.0 1.3 44.0 1.5 49.0 2.8 50.0 3.1 51.0 3.5 52.0 1.1 53.0 11.0 54.0 19.3 55.0 100.0 56.0 4.7 62.0 27.3 63.0 1.3 64.0 9.2 75.0 6.7 77.0 2.2 90.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H7 Cl 0.05 ml : 0.5 ml CDCl3 (chloromethyl)cyclopropane 
Assign. Shift(ppm)
A 3.437 B 1.233 C 0.674 D 0.346
Hz ppm Int.1377.44 3.447 963 1370.00 3.429 1000 512.82 1.284 31 508.06 1.272 60 505.37 1.265 73 504.88 1.264 69 503.30 1.260 46 500.61 1.253 136 500.00 1.252 138 497.44 1.245 117 495.85 1.241 95 495.36 1.240 85 492.68 1.233 228 489.50 1.225 93 487.79 1.221 125 485.23 1.215 133 484.62 1.213 162 482.06 1.207 45 479.86 1.201 90 477.29 1.195 69 472.53 1.183 36 279.17 0.699 153 274.41 0.687 392 273.19 0.684 473 272.22 0.682 306 268.68 0.673 189 268.19 0.672 196 266.48 0.667 450 265.14 0.664 407 264.28 0.662 318 260.25 0.652 181 253.66 0.635 36 146.85 0.368 176 142.21 0.356 485 140.99 0.353 427 138.43 0.347 240 137.45 0.344 399 136.11 0.341 520 131.59 0.330 136 131.23 0.329 138 130.86 0.328 137
in CDCl3
liquid film
4880 A,200 M,liquid
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