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网站主页CAS数据库列表 589-35-5更多图谱3-甲基-1-戊醇(589-35-5)核磁图(1HNMR)

3-甲基-1-戊醇

产品名称 3-甲基-1-戊醇

CAS号589-35-5

分子式C6H14O

分子量102.17

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  • Mass

    MS-NW-3063          
    3-methyl-1-pentanol
    C6H14O              (Mass of molecular ion:    102)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       1.2
          18.0       1.4
          19.0       1.0
          26.0       1.1
          27.0      15.8
          28.0       4.4
          29.0      27.9
          31.0      23.8
          39.0      11.1
          40.0       1.8
          41.0      52.7
          42.0      16.0
          43.0      55.2
          44.0       2.4
          45.0      11.9
          46.0       3.2
          53.0       3.0
          54.0       2.0
          55.0      67.0
          56.0     100.0
          57.0      26.2
          58.0       1.1
          59.0       2.0
          67.0       1.3
          69.0      61.7
          70.0       4.9
          71.0       4.4
          73.0       1.2
          83.0       2.3
          84.0      16.6
          85.0       1.6
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H14 O 0.04 ml : 0.5 ml CDCl3
    3-methyl-1-pentanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.66 B 1.983 C 1.81 to 1.04 D 0.89 E 0.89

         Hz     ppm     Int.
    

        335.25   3.744     90
        334.69   3.738    110
        331.31   3.700     41
        328.94   3.673    177
        328.00   3.663    182
        321.56   3.591    135
        177.56   1.983   1000
        150.00   1.675     36
        142.63   1.593     46
        142.13   1.587     46
        140.56   1.570     57
        139.06   1.553     54
        136.13   1.520     64
        132.94   1.485     96
        131.69   1.471    104
        130.56   1.458     69
        128.94   1.440     76
        128.81   1.439     76
        127.69   1.426     57
        124.88   1.395     96
        124.19   1.387    100
        122.50   1.368     70
        120.88   1.350     43
        119.13   1.331     62
        117.44   1.312     86
        116.25   1.299     90
        111.81   1.249     63
        110.81   1.238     54
        109.94   1.228     78
        106.19   1.186     43
        103.81   1.160     45
        102.63   1.146     38
         97.19   1.086     36
         85.13   0.951    227
         82.75   0.924    376
         79.13   0.884    314
         78.56   0.878    304
         77.81   0.869    335
         76.94   0.860    410
         72.94   0.815     82
         71.44   0.798     95
         68.88   0.770     59
    

in CDCl3



liquid film



4880 A,200 M,liquid