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MS-IW-9209 tert-butyl (3-hydroxypropyl)carbamate C8H17NO3 (Mass of molecular ion: 175)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.4 17.0 1.2 18.0 10.9 26.0 1.1 27.0 6.1 28.0 12.4 29.0 18.0 30.0 47.2 31.0 10.9 38.0 1.0 39.0 9.7 40.0 2.4 41.0 43.8 42.0 3.3 43.0 7.2 44.0 17.6 45.0 2.1 46.0 1.1 53.0 1.3 55.0 5.8 56.0 18.2 57.0 100.0 58.0 9.6 59.0 35.5 60.0 1.2 74.0 9.1 75.0 4.4 76.0 12.0 84.0 2.4 89.0 3.8 101.0 4.4 102.0 8.6 116.0 1.2 118.0 2.3 119.0 9.3 120.0 5.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H17 N O3 0.05 ml : 0.5 ml CDCl3 tert-butyl (3-hydroxypropyl)carbamate Assign. Shift(ppm)
A 5.27 B 3.85 C 3.651 D 3.250 E 1.678 F 1.440
Hz ppm Int.
2105.22 5.268 31 1546.02 3.869 27 1540.53 3.855 52 1534.79 3.841 33 1467.65 3.673 53 1462.04 3.659 114 1456.30 3.644 107 1450.56 3.630 41 1310.18 3.279 38 1304.08 3.264 90 1297.85 3.248 92 1291.63 3.232 43 682.74 1.709 31 676.88 1.694 82 670.78 1.679 105 664.67 1.664 74 658.69 1.649 24 575.44 1.440 1000
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