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网站主页CAS数据库列表 588-96-5更多图谱4-溴苯乙醚(588-96-5)质谱(MS)

4-溴苯乙醚

产品名称 4-溴苯乙醚

CAS号588-96-5

分子式C8H9BrO

分子量201.06

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  • Mass

    MS2015-05280CW      
    p-bromophenetole
    C8H9BrO             (Mass of molecular ion:    200)
    

       Source Temperature: 250 °C
       Sample Temperature: 250 °C
       Reservoir, 70 eV
    

          27.0       2.0
          29.0       3.0
          38.0       2.1
          39.0       4.3
          50.0       3.2
          51.0       1.1
          62.0       2.3
          63.0       7.5
          64.0       4.4
          65.0      17.4
          66.0       1.1
          74.0       2.1
          75.0       4.2
          76.0       3.6
          77.0       1.6
          91.0       1.1
          92.0       1.8
          93.0      20.0
          94.0       1.6
         117.0       1.8
         119.0       1.7
         120.0       1.1
         143.0       4.0
         145.0       4.0
         155.0       2.7
         157.0       2.8
         171.0       1.1
         172.0     100.0
         173.0       7.6
         174.0      97.9
         175.0       6.5
         200.0      43.9
         201.0       4.0
         202.0      43.0
         203.0       3.8
    

in DMSO-d6

400 MHz in CDCl3

90 MHz in CDCl3




  • 1H NMR 399.65 MHz
    C8 H9 Br O 0.05 ml : 0.5 ml CDCl3
    p-bromophenetole
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.329 B 6.732 C 3.937 D 1.371

         Hz     ppm     Int.
    

       2937.13   7.350     87
       2933.84   7.342    649
       2931.52   7.336    218
       2929.32   7.330     33
       2927.00   7.324    234
       2925.29   7.320    275
       2924.68   7.319    666
       2921.39   7.310     83
       2698.36   6.752     79
       2695.07   6.744    543
       2692.75   6.738    180
       2688.23   6.727    183
       2685.91   6.721    491
       2682.62   6.713     62
       1584.11   3.964    194
       1577.15   3.947    524
       1570.19   3.929    523
       1563.11   3.912    197
        555.05   1.389    626
        552.49   1.383     34
        548.10   1.372   1000
        542.85   1.359     49
        541.14   1.355    588
    


  • 1H NMR 89.56 MHz
    C8 H9 Br O 0.04 ml : 0.5 ml CDCl3
    p-bromophenetole
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.336 B 6.750 C 3.965 D 1.386

         Hz     ppm     Int.
    

        665.69   7.433     34
        662.38   7.396    444
        660.13   7.371    141
        655.63   7.321    150
        653.31   7.295    615
        650.00   7.258     66
        611.88   6.833     51
        608.63   6.796    536
        606.31   6.770    143
        601.81   6.720    115
        599.50   6.694    384
        596.25   6.658     36
        366.00   4.087    127
        359.00   4.009    422
        352.00   3.931    445
        345.06   3.853    154
        130.94   1.463    506
        124.00   1.385   1000
        117.00   1.307    445
    

in CDCl3

in DMSO-d6





liquid film



4880 A,200 M,liquid