4-吡啶甲醇

Mass

MS-NW-2616          
4-pyridinemethanol
C6H7NO              (Mass of molecular ion:    109)

   Source Temperature: 270 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      26.0       4.8
      27.0       9.2
      28.0       6.8
      29.0       7.0
      31.0       9.2
      37.0       3.5
      38.0       5.4
      39.0      17.7
      40.0       1.8
      41.0       2.0
      43.0       1.5
      49.0       3.1
      50.0      16.7
      51.0      34.3
      52.0      21.7
      53.0      29.7
      54.0       8.6
      55.0       3.7
      61.0       1.3
      62.0       2.2
      63.0       6.7
      64.0       6.6
      65.0       8.5
      66.0       1.3
      75.0       1.3
      76.0       1.1
      78.0      15.0
      79.0      11.7
      80.0      94.5
      81.0      10.9
      82.0       1.4
      91.0       5.9
      92.0       4.4
      93.0       2.1
     106.0       3.8
     107.0       5.7
     108.0      70.8
     109.0     100.0
     110.0       7.1

Parameter ppm Hz D(A) 8.66 D(B) 7.52 D(C) 4.74 J(A,A') 0.4 J(A,B) 5.0 J(A,B') 0.8 J(A,C) 0.0 J(A',B) 0.8 J(A',B') 5.0 J(A',C) 0.0 J(B,B') 1.4 J(B,C) 0.7 J(B',C) 0.7 D(D) 5.18 BRUEGEL,W. Z.ELEKTROCHEM.(BER.BUNSENGES.PHYS.CHEM.) 66, 159 (1962)

     Hz     ppm     Int.

   2600.91   8.670    501
   2599.59   8.665    302
   2596.47   8.655    301
   2595.15   8.650    520
   2258.85   7.529    380
   2253.20   7.511    369
   1554.00   5.180    746
   1422.02   4.740   1000