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网站主页CAS数据库列表 586-95-8更多图谱4-吡啶甲醇(586-95-8)质谱(MS)

4-吡啶甲醇

产品名称 4-吡啶甲醇

CAS号586-95-8

分子式C6H7NO

分子量109.13

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  • Mass

    MS-NW-2616          
    4-pyridinemethanol
    C6H7NO              (Mass of molecular ion:    109)
    

       Source Temperature: 270 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          26.0       4.8
          27.0       9.2
          28.0       6.8
          29.0       7.0
          31.0       9.2
          37.0       3.5
          38.0       5.4
          39.0      17.7
          40.0       1.8
          41.0       2.0
          43.0       1.5
          49.0       3.1
          50.0      16.7
          51.0      34.3
          52.0      21.7
          53.0      29.7
          54.0       8.6
          55.0       3.7
          61.0       1.3
          62.0       2.2
          63.0       6.7
          64.0       6.6
          65.0       8.5
          66.0       1.3
          75.0       1.3
          76.0       1.1
          78.0      15.0
          79.0      11.7
          80.0      94.5
          81.0      10.9
          82.0       1.4
          91.0       5.9
          92.0       4.4
          93.0       2.1
         106.0       3.8
         107.0       5.7
         108.0      70.8
         109.0     100.0
         110.0       7.1
    

parameter in DMSO-d6


  • 1H NMR 300 MHz
    C6 H7 N O 30 % in DMSO
    4-pyridinemethanol
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 8.66 D(B) 7.52 D(C) 4.74 J(A,A') 0.4 J(A,B) 5.0 J(A,B') 0.8 J(A,C) 0.0 J(A',B) 0.8 J(A',B') 5.0 J(A',C) 0.0 J(B,B') 1.4 J(B,C) 0.7 J(B',C) 0.7 D(D) 5.18 BRUEGEL,W. Z.ELEKTROCHEM.(BER.BUNSENGES.PHYS.CHEM.) 66, 159 (1962)

         Hz     ppm     Int.
    

       2600.91   8.670    501
       2599.59   8.665    302
       2596.47   8.655    301
       2595.15   8.650    520
       2258.85   7.529    380
       2253.20   7.511    369
       1554.00   5.180    746
       1422.02   4.740   1000
    

in DMSO-d6



KBr disc



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