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网站主页CAS数据库列表 5858-18-4更多图谱2,5-二氯苯硫酚(5858-18-4)红外图谱(IR1)

2,5-二氯苯硫酚

产品名称 2,5-二氯苯硫酚

CAS号5858-18-4

分子式C6H4Cl2S

分子量179.07

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  • Mass

    MS-NW-5891          
    2,5-dichlorobenzenethiol
    C6H4Cl2S            (Mass of molecular ion:    178)
    

       Source Temperature: 280 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          36.0       2.1
          37.0       3.0
          38.0       2.3
          39.0       1.9
          44.0       1.3
          45.0       5.4
          49.0       1.5
          50.0       3.5
          52.5       1.2
          53.0       5.3
          53.5       1.3
          54.0       1.0
          57.0       1.3
          58.0       2.0
          61.0       3.6
          62.0       4.7
          63.0      10.5
          68.0       1.0
          69.0      12.9
          70.0       1.1
          71.0       6.8
          71.5       1.0
          72.0       3.4
          73.0       5.0
          74.0       5.4
          75.0       4.1
          79.0       4.2
          81.0       3.6
          82.0       4.7
          83.0       1.0
          84.0       1.7
          85.0       1.1
          89.0       3.8
          90.0       2.4
          92.0       1.3
          93.0       1.1
          97.0       2.1
          99.0       5.1
         101.0       1.5
         103.0       1.2
         105.0       1.7
         106.0       2.7
         107.0      16.0
         108.0      16.0
         109.0       4.8
         110.0       1.8
         111.0       2.0
         118.0       2.8
         120.0       1.1
         133.0       2.6
         134.0       3.8
         135.0       1.9
         136.0       2.6
         142.0      25.7
         143.0      57.8
         144.0      14.1
         145.0      23.2
         146.0       5.8
         147.0       2.1
         148.0       2.8
         177.0       5.4
         178.0     100.0
         179.0      11.7
         180.0      68.4
         181.0       5.9
         182.0      13.5
         183.0       1.1
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H4 Cl2 S 0.04 ml : 0.5 ml CDCl3
    2,5-dichlorobenzenethiol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.31 B 7.25 C 7.04 D 3.92 J(A,B)=0.4HZ. J(A,C)=2.3HZ. J(B,C)=8.5HZ.

         Hz     ppm     Int.
    

        655.88   7.324    455
        655.44   7.319    393
        654.63   7.310    275
        653.50   7.297    466
        653.13   7.293    508
        646.19   7.216    488
        633.94   7.079    482
        632.88   7.067     28
        631.63   7.053    378
        625.44   6.984    206
        623.06   6.957    182
        351.25   3.922   1000
        350.19   3.911     36
        349.81   3.906     37
    

in CDCl3



liquid film