-
MassMS-IW-0025 2-methoxy-3-dibenzofuranamine C13H11NO2 (Mass of molecular ion: 213)
Source Temperature: 180 °C Sample Temperature: 100 °C Direct, 75 eV
70.5 1.8 77.0 1.0 85.0 4.5 106.5 4.5 114.0 1.3 115.0 5.9 116.0 1.1 127.0 1.9 140.0 1.1 155.0 1.7 156.0 1.2 169.0 1.2 170.0 31.1 171.0 4.2 182.0 1.3 183.0 1.0 184.0 1.4 198.0 84.2 199.0 11.5 200.0 1.1 212.0 1.1 213.0 100.0 214.0 14.7 215.0 1.4
400 MHz in CDCl3
-
1H NMR 399.65 MHz C13 H11 N O2 0.032 g : 0.5 ml CDCl3 2-methoxy-3-dibenzofuranamine 
Assign. Shift(ppm)
A 7.755 B 7.460 C *1 7.29 D *1 7.25 E 7.240 F 6.880 G 4.0 J 3.927
Hz ppm Int.3103.39 7.766 94 3102.42 7.763 87 3101.56 7.761 74 3096.31 7.748 111 3094.97 7.745 96 2986.69 7.474 93 2985.72 7.471 102 2979.61 7.456 93 2978.15 7.452 119 2922.24 7.312 47 2920.65 7.309 51 2914.92 7.294 113 2913.33 7.290 102 2907.23 7.275 111 2905.27 7.270 164 2903.81 7.266 112 2897.83 7.251 135 2896.61 7.248 134 2893.55 7.241 334 2890.50 7.233 66 2889.28 7.230 55 2887.70 7.226 53 2749.63 6.881 353 1569.58 3.928 1000
in CDCl3
KBr disc
nujol mull
更多供应商
