2-溴-4-甲基苯胺

Mass

MS-NW-1580          
2-bromo-p-toluidine
C7H8BrN             (Mass of molecular ion:    185)

   Source Temperature: 240 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      18.0       1.2
      26.0       1.5
      27.0       4.9
      28.0       5.6
      30.0       2.2
      37.0       1.8
      38.0       3.5
      39.0       7.1
      39.5       1.4
      40.0       1.7
      41.0       2.0
      42.0       1.3
      49.0       1.2
      50.0       7.2
      51.0      16.2
      51.5       2.6
      52.0      15.5
      52.5      11.4
      53.0      15.4
      54.0       2.6
      61.0       1.4
      62.0       2.8
      63.0       4.8
      64.0       1.8
      65.0       3.0
      66.0       1.9
      74.0       1.7
      75.0       2.0
      76.0       3.2
      77.0      24.6
      78.0      15.9
      79.0      15.5
      80.0       2.6
      89.0       1.8
      91.0       1.2
      92.5       2.9
      93.5       2.6
     104.0      17.5
     105.0      13.3
     106.0      92.9
     107.0       9.1
     184.0      44.0
     185.0     100.0
     186.0      49.3
     187.0      96.5
     188.0       7.6

Assign. Shift(ppm) A 7.213 B 6.877 C 6.647 D 3.87 E 2.202

     Hz     ppm     Int.

    647.25   7.228    127
    646.56   7.220    179
    645.69   7.210    158
    645.31   7.206    149
    644.94   7.202    149
    622.56   6.952     71
    621.88   6.944     70
    621.25   6.937     46
    620.63   6.930     62
    620.00   6.923     57
    615.06   6.868     46
    614.50   6.862    127
    613.81   6.854    133
    613.19   6.847     88
    612.56   6.840    124
    611.88   6.833    120
    611.31   6.826     47
    598.00   6.678    315
    589.94   6.588    157
    346.69   3.872    509
    197.19   2.202   1000