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网站主页CAS数据库列表 582-22-9更多图谱3-甲基苯乙胺(582-22-9)红外图谱(IR1)

3-甲基苯乙胺

产品名称 3-甲基苯乙胺

CAS号582-22-9

分子式C9H13N

分子量135.21

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  • Mass

    MS-IW-4182          
    beta-methylphenethylamine
    C9H13N              (Mass of molecular ion:    135)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          39.0       1.4
          41.0       2.3
          42.0      28.5
          43.0       1.2
          51.0       2.9
          58.0      14.7
          60.0       2.3
          65.0       1.2
          77.0       6.0
          78.0       2.1
          79.0       4.5
          91.0       6.4
          92.0       1.9
         103.0       2.7
         104.0       3.3
         115.0       1.2
         117.0       1.9
         118.0       2.0
         119.0       2.3
         120.0     100.0
         121.0       9.6
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H13 N 0.05 ml : 0.5 ml CDCl3
    beta-methylphenethylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.28 B 7.18 C 7.18 D *1 2.81 E *1 2.79 F 2.71 G 1.224 J 1.2 J(F,G) = 6.8 HZ.

         Hz     ppm     Int.
    

       2922.24   7.312     39
       2919.92   7.307    167
       2918.46   7.303     84
       2916.14   7.297     49
       2914.55   7.293    141
       2913.09   7.290    228
       2912.35   7.288    294
       2911.38   7.285    252
       2908.45   7.278     85
       2907.47   7.276     53
       2905.27   7.270    303
       2904.79   7.269    306
       2903.20   7.265     94
       2879.52   7.206     72
       2877.93   7.202    142
       2876.95   7.199    189
       2873.66   7.191    335
       2872.19   7.187    425
       2870.36   7.183    330
       2866.94   7.174    155
       2864.50   7.168    367
       1124.39   2.814    261
       1117.43   2.797    428
       1099.00   2.750     31
       1092.29   2.734     92
       1085.45   2.717    147
       1078.61   2.699    135
       1071.66   2.682     67
        492.43   1.233    964
        485.60   1.216   1000
    


  • 1H NMR 89.56 MHz
    C9 H13 N 0.04 ml : 0.5 ml CDCl3
    beta-methylphenethylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.32 to 7.11 B 3.01 to 2.48 C 1.244 D 1.12 400MHZ. : HSP-41-321

         Hz     ppm     Int.
    

        665.00   7.426     33
        662.19   7.394     86
        661.06   7.382     31
        660.63   7.377     39
        659.31   7.362     82
        656.81   7.334     93
        654.50   7.308    319
        653.69   7.299    151
        652.19   7.283    111
        651.19   7.271    166
        649.56   7.253   1000
        647.94   7.235    801
        647.13   7.226    980
        643.75   7.188    181
        642.38   7.173    123
        641.81   7.167     83
        640.94   7.157    119
        639.69   7.143    111
        638.81   7.133     53
        638.31   7.128     58
        636.19   7.104     32
        635.06   7.091     43
        633.69   7.076     44
        259.56   2.899     60
        256.69   2.867    101
        255.44   2.853    107
        254.31   2.840    242
        251.75   2.811    647
        248.75   2.778    101
        246.63   2.754    146
        244.63   2.732     48
        241.75   2.700     75
        240.06   2.681     60
        237.94   2.657     50
        234.50   2.619     33
        233.13   2.604     36
        232.56   2.597     33
        114.81   1.282    906
        113.00   1.262    293
        110.00   1.229    229
        108.13   1.208    875
        106.00   1.184     61
        105.13   1.174     50
        100.38   1.121    639
         94.75   1.058     38
    

in CDCl3



liquid film



4880 A,200 M,liquid