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MassMS-NW-7293 2,3'-bipyridine C10H8N2 (Mass of molecular ion: 156)
Source Temperature: 200 °C Sample Temperature: 190 °C Reservoir, 75 eV
26.0 1.1 27.0 1.2 38.0 1.2 39.0 2.0 50.0 7.6 51.0 11.9 52.0 5.8 53.0 1.0 62.0 1.4 63.0 2.1 64.0 2.3 64.5 2.9 65.0 1.1 74.0 2.9 75.0 4.2 76.0 5.2 77.0 4.3 78.0 16.5 79.0 10.3 101.0 3.1 102.0 3.3 103.0 2.4 104.0 9.8 105.0 1.2 128.0 10.3 129.0 6.4 130.0 21.9 131.0 2.4 155.0 68.7 156.0 100.0 157.0 11.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H8 N2 0.05 ml : 0.5 ml CDCl3 2,3'-bipyridine 
Assign. Shift(ppm)
A 9.208 B 8.686 C 8.628 D 8.287 E 7.726 F 7.702 G 7.361 J 7.240
Hz ppm Int.3681.49 9.212 668 3680.88 9.211 679 3679.35 9.207 661 3475.49 8.697 497 3474.43 8.694 542 3473.66 8.692 557 3472.75 8.690 471 3470.61 8.685 499 3469.54 8.682 555 3468.93 8.680 566 3467.86 8.678 454 3451.69 8.637 516 3450.01 8.633 523 3446.81 8.625 528 3445.28 8.621 502 3318.02 8.303 483 3316.35 8.299 558 3315.73 8.297 526 3314.06 8.293 444 3310.09 8.283 500 3308.41 8.279 557 3307.80 8.277 541 3306.12 8.273 434 3098.60 7.754 272 3096.77 7.749 242 3091.58 7.736 310 3090.67 7.734 715 3089.90 7.732 346 3088.84 7.729 663 3083.65 7.716 847 3081.97 7.712 1000 3081.36 7.711 874 3080.29 7.708 895 3079.68 7.706 931 3078.61 7.704 791 3073.27 7.690 302 3072.36 7.688 325 3071.75 7.687 242 3070.68 7.684 172 2948.61 7.378 482 2947.85 7.377 472 2943.88 7.367 501 2942.96 7.364 482 2940.67 7.359 488 2939.91 7.357 449 2935.94 7.347 455 2935.03 7.345 450 2900.24 7.257 488 2898.56 7.253 458 2895.36 7.245 493 2893.68 7.241 584 2893.22 7.240 596 2891.54 7.236 458 2888.49 7.228 464 2886.81 7.224 412
in CDCl3
liquid film
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