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MassMS-NW-6711 6-nitro-o-toluidine C7H8N2O2 (Mass of molecular ion: 152)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 1.7 27.0 4.3 28.0 7.3 30.0 2.7 37.0 1.6 38.0 3.0 39.0 10.6 40.0 1.3 41.0 2.8 42.0 2.1 44.0 1.1 50.0 5.0 51.0 12.1 52.0 10.9 53.0 7.8 54.0 3.3 62.0 1.6 63.0 4.4 64.0 2.6 65.0 5.8 66.0 4.5 67.0 2.3 74.0 1.3 75.0 1.6 76.0 3.2 77.0 43.4 78.0 12.6 79.0 37.0 80.0 5.0 89.0 1.8 90.0 2.4 91.0 5.7 92.0 1.2 93.0 2.2 94.0 9.5 103.0 2.1 104.0 15.9 105.0 14.4 106.0 40.9 107.0 4.1 116.0 5.9 117.0 5.5 118.0 1.1 122.0 4.3 134.0 3.4 135.0 9.1 136.0 2.3 151.0 1.0 152.0 100.0 153.0 8.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H8 N2 O2 0.043 g : 0.5 ml CDCl3 6-nitro-o-toluidine 
Assign. Shift(ppm)
A 8.007 B 7.268 C 6.620 D 6.14 E 2.235
Hz ppm Int.722.69 8.070 89 722.13 8.064 93 721.13 8.052 99 720.56 8.046 87 714.00 7.973 101 713.50 7.967 104 712.44 7.955 112 711.88 7.949 97 655.94 7.325 84 655.13 7.315 100 654.31 7.306 105 653.50 7.297 79 649.63 7.254 45 648.81 7.245 108 648.00 7.236 133 647.19 7.227 126 646.38 7.218 93 600.19 6.702 154 593.06 6.622 124 591.50 6.605 141 584.38 6.526 108 200.13 2.235 1000
in CDCl3
KBr disc
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