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MassMS-NW-9359 4-bromo-2,6-diethylaniline C10H14BrN (Mass of molecular ion: 227)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.3 28.0 4.6 29.0 1.0 30.0 1.5 39.0 4.6 41.0 2.3 42.0 1.7 50.0 1.6 51.0 5.7 52.0 3.5 53.0 2.9 54.0 1.8 58.5 6.1 59.0 1.7 59.5 2.7 62.0 1.2 63.0 3.6 64.0 1.7 64.5 3.0 65.0 7.5 65.5 6.3 66.0 2.9 66.5 4.4 67.0 1.1 71.5 1.0 72.5 1.2 74.0 1.3 75.0 1.7 76.0 1.8 77.0 7.7 78.0 3.6 79.0 2.2 89.0 3.2 90.0 2.7 91.0 10.2 92.0 2.1 93.0 1.5 98.5 3.3 99.5 3.2 102.0 2.6 103.0 4.1 104.0 3.8 105.0 3.3 106.0 3.2 115.0 9.0 116.0 7.9 117.0 11.9 118.0 9.5 119.0 7.3 120.0 4.9 127.0 1.1 128.0 2.7 129.0 2.8 130.0 10.2 131.0 7.0 132.0 25.6 133.0 71.8 134.0 7.9 146.0 1.4 147.0 5.7 148.0 10.8 149.0 1.5 162.0 1.1 184.0 1.2 197.0 2.1 198.0 3.3 199.0 2.0 200.0 2.6 210.0 1.4 212.0 100.0 213.0 11.2 214.0 96.6 215.0 10.3 226.0 2.4 227.0 85.4 228.0 12.0 229.0 83.6 230.0 9.6
90 MHz in CDCl3
in CDCl3
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1H NMR 89.56 MHz C10 H14 Br N 0.05 ml : 0.5 ml CDCl3 4-bromo-2,6-diethylaniline 
Assign. Shift(ppm)
A 7.048 B 3.58 C 2.448 D 1.219
Hz ppm Int.631.06 7.047 465 320.63 3.581 79 231.25 2.583 88 230.81 2.578 88 228.25 2.549 29 223.38 2.495 299 215.88 2.411 341 211.75 2.365 36 208.75 2.331 133 116.00 1.296 488 108.75 1.215 1000 104.19 1.164 58 101.06 1.129 360
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in CDCl3
liquid film
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