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MS-NW-0832 3-chloro-2-methylpropene C4H7Cl (Mass of molecular ion: 90)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 3.8 27.0 19.2 28.0 5.9 29.0 22.9 36.0 1.2 37.0 3.2 38.0 5.5 39.0 45.3 40.0 5.6 41.0 19.2 49.0 3.8 50.0 5.7 51.0 5.5 52.0 1.8 53.0 18.2 54.0 26.7 55.0 100.0 56.0 4.9 62.0 4.6 64.0 1.5 75.0 10.4 77.0 3.4 90.0 31.6 91.0 1.7 92.0 10.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H7 Cl 0.05 ml : 0.5 ml CDCl3 3-chloro-2-methylpropene Assign. Shift(ppm)
A 5.067 B 4.939 C 4.009 D 1.848
Hz ppm Int.
2027.10 5.073 206 2026.25 5.071 330 2025.39 5.068 365 2024.66 5.067 358 2023.80 5.064 297 2022.83 5.062 162 1977.05 4.947 147 1975.59 4.944 368 1974.12 4.940 472 1972.53 4.936 326 1971.07 4.932 104 1611.69 4.033 23 1602.78 4.011 984 1601.68 4.008 905 739.87 1.852 993 738.89 1.849 1000 738.28 1.848 979 737.43 1.846 888
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