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MassMS-NW-7027 N,N'-diacetylsulfanilamide C10H12N2O4S (Mass of molecular ion: 256)
Source Temperature: 220 °C Sample Temperature: 210 °C Direct, 75 eV
15.0 6.2 18.0 1.7 28.0 1.8 38.0 2.3 39.0 6.6 40.0 1.1 41.0 2.6 42.0 6.8 43.0 100.0 44.0 2.7 50.0 2.1 51.0 1.8 52.0 3.0 53.0 2.2 62.0 1.8 63.0 7.8 64.0 7.3 65.0 25.7 66.0 3.0 75.0 1.3 76.0 1.8 77.0 1.6 78.0 1.3 79.0 2.0 80.0 4.0 81.0 1.5 90.0 2.6 91.0 10.2 92.0 27.2 93.0 6.6 104.0 1.1 105.0 1.4 106.0 2.3 107.0 5.0 108.0 20.8 109.0 83.2 110.0 6.3 134.0 10.0 135.0 2.0 140.0 3.4 150.0 2.4 151.0 72.6 152.0 6.9 155.0 2.9 156.0 29.7 157.0 2.7 158.0 1.7 172.0 19.5 173.0 5.8 174.0 1.4 192.0 5.2 198.0 4.0 214.0 4.6 256.0 9.0 257.0 1.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H12 N2 O4 S 0.040 g : 0.5 ml DMSO-d6 N,N'-diacetylsulfanilamide 
Assign. Shift(ppm)
A *1 12.0 B *1 10.4 C 7.859 D 7.800 E *2 2.106 F *2 1.924
Hz ppm Int.4795.48 12.000 33 4159.89 10.409 134 3149.36 7.881 24 3147.17 7.875 169 3145.15 7.870 67 3140.21 7.858 88 3138.19 7.853 351 3135.99 7.847 64 3123.17 7.815 60 3120.97 7.810 314 3118.96 7.805 89 3114.01 7.792 62 3112.00 7.787 160 841.83 2.107 871 769.30 1.925 1000
in DMSO-d6
KBr disc
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