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MassMS-NW-7852 3,5-dibromo-2-biphenylol C12H8Br2O (Mass of molecular ion: 326)
Source Temperature: 170 °C Sample Temperature: 130 °C Direct, 75 eV
39.0 2.7 50.0 1.7 51.0 2.8 62.0 3.2 63.0 6.1 65.0 1.6 69.0 4.6 69.5 13.9 70.0 6.6 74.0 2.3 75.0 2.4 76.0 1.2 77.0 1.8 83.0 1.0 84.0 15.3 84.5 2.0 86.0 2.4 87.0 3.8 88.0 2.3 89.0 4.6 98.0 1.1 99.0 1.2 102.0 1.1 109.5 1.2 110.0 1.4 111.0 1.1 113.0 4.1 114.0 3.1 115.0 1.8 123.0 1.6 123.5 3.3 124.0 1.8 124.5 3.1 137.0 2.7 138.0 5.1 139.0 44.7 140.0 14.2 141.0 1.5 150.0 1.0 164.0 1.8 167.0 1.7 168.0 30.2 169.0 4.1 217.0 1.1 219.0 5.7 221.0 4.9 246.0 9.8 247.0 2.6 248.0 10.3 249.0 2.3 325.0 3.6 326.0 51.5 327.0 13.7 328.0 100.0 329.0 16.4 330.0 48.8 331.0 6.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C12 H8 Br2 O 0.034 g : 0.5 ml CDCl3 3,5-dibromo-2-biphenylol 
Assign. Shift(ppm)
A 7.593 B 7.45 C 7.373 D 5.636 J(C,D)=0.3HZ
Hz ppm Int.681.38 7.609 415 679.06 7.583 514 676.81 7.558 61 676.25 7.551 61 675.81 7.546 62 675.00 7.537 73 673.88 7.525 128 669.75 7.479 297 666.88 7.447 1000 664.13 7.416 330 661.63 7.388 379 661.25 7.384 372 659.25 7.361 309 658.88 7.357 309 657.19 7.338 68 505.00 5.639 491 504.63 5.635 488
in CDCl3
KBr disc
nujol mull
