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MassMS-NW-1720 (p-nitrophenyl)acetonitrile C8H6N2O2 (Mass of molecular ion: 162)
Source Temperature: 250 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 3.7 26.0 1.3 27.0 2.2 28.0 2.7 30.0 19.2 37.0 3.3 38.0 6.2 39.0 19.1 40.0 1.7 41.0 1.1 44.0 1.5 46.0 1.5 49.0 1.4 50.0 19.5 51.0 12.3 52.0 3.2 61.0 3.9 62.0 11.0 63.0 29.7 64.0 8.0 65.0 5.4 66.0 1.6 73.0 1.0 74.0 6.0 75.0 5.9 76.0 6.9 77.0 18.7 78.0 3.6 85.0 1.0 86.0 2.0 87.0 3.6 88.0 6.7 89.0 87.3 90.0 16.5 91.0 1.1 102.0 1.6 103.0 1.5 104.0 22.5 105.0 2.4 114.0 3.5 115.0 3.7 116.0 100.0 117.0 9.4 132.0 25.4 133.0 2.3 146.0 1.8 162.0 64.6 163.0 6.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H6 N2 O2 0.042 g : 0.5 ml CDCl3 (p-nitrophenyl)acetonitrile 
Assign. Shift(ppm)
A 8.252 B 7.564 C 3.918
Hz ppm Int.748.25 8.355 32 746.38 8.334 85 743.94 8.307 465 741.88 8.284 166 739.56 8.258 57 737.19 8.232 216 735.13 8.209 593 732.63 8.181 91 683.50 7.632 101 681.19 7.606 495 679.00 7.582 159 676.69 7.556 52 674.31 7.530 159 672.88 7.514 308 672.19 7.506 368 669.81 7.479 59 357.06 3.987 30 350.88 3.918 1000 345.88 3.862 25
in CDCl3
KBr disc
nujol mull
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