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MassMS-NW-6597 2'-hydroxy-4'-methoxyacetophenone C9H10O3 (Mass of molecular ion: 166)
Source Temperature: 220 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.2 18.0 2.7 27.0 1.1 28.0 1.5 38.0 1.3 39.0 2.9 41.0 1.7 43.0 7.9 50.0 1.5 51.0 3.3 52.0 2.8 53.0 2.3 55.0 1.4 62.0 1.1 63.0 2.1 64.0 1.1 65.0 2.9 66.0 1.0 69.0 3.1 77.0 1.9 79.0 1.8 80.0 2.0 93.0 1.6 95.0 6.5 108.0 6.4 123.0 1.4 151.0 100.0 152.0 8.7 153.0 1.0 166.0 43.4 167.0 4.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H10 O3 0.043 g : 0.5 ml CDCl3 2'-hydroxy-4'-methoxyacetophenone 
Assign. Shift(ppm)
A 12.73 B 7.613 C 6.43 D 6.41 E 3.827 F 2.542
Hz ppm Int.1140.15 12.731 318 687.01 7.671 77 680.69 7.601 22 677.61 7.566 89 581.82 6.497 64 579.26 6.468 131 575.07 6.422 92 572.94 6.398 127 572.08 6.388 160 569.52 6.360 27 342.82 3.828 893 227.72 2.543 1000
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
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