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MassMS-IW-8207 bis(oxiranylmethyl) 1,2-cyclohexanedicarboxylate C14H20O6 (Mass of molecular ion: 284)
Source Temperature: 160 °C Sample Temperature: 120 °C Direct, 75 eV
15.0 2.2 17.0 1.1 18.0 4.6 26.0 4.0 27.0 17.7 28.0 8.5 29.0 31.2 31.0 17.2 39.0 5.2 40.0 1.6 41.0 9.8 42.0 1.2 43.0 6.4 44.0 2.3 45.0 2.4 51.0 1.2 52.0 1.1 53.0 4.9 54.0 7.5 55.0 13.8 56.0 12.0 57.0 82.7 58.0 4.1 65.0 1.0 66.0 5.1 67.0 15.0 68.0 3.5 69.0 1.5 71.0 1.0 73.0 2.4 74.0 1.1 75.0 2.8 77.0 3.0 78.0 1.8 79.0 12.8 80.0 48.8 81.0 100.0 82.0 17.5 83.0 2.1 87.0 1.4 93.0 1.2 94.0 2.6 95.0 1.4 97.0 2.4 99.0 1.9 100.0 1.1 107.0 2.6 108.0 20.1 109.0 55.0 110.0 5.4 111.0 1.0 116.0 11.3 117.0 2.3 119.0 2.6 124.0 3.4 125.0 8.8 126.0 4.5 127.0 5.9 129.0 33.0 130.0 3.1 136.0 2.6 137.0 1.2 142.0 1.2 143.0 1.7 153.0 2.4 154.0 3.6 155.0 20.2 156.0 4.2 167.0 1.0 168.0 2.0 169.0 2.1 181.0 2.5 182.0 38.6 183.0 51.3 184.0 12.0 185.0 1.4 197.0 3.0 210.0 10.7 211.0 86.7 212.0 11.1 213.0 1.4 227.0 2.1 229.0 6.7 230.0 1.8 255.0 4.0 256.0 1.2 283.0 3.4 284.0 14.3 285.0 5.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H20 O6 0.05 ml : 0.5 ml CDCl3 bis(oxiranylmethyl) 1,2-cyclohexanedicarboxylate 
Assign. Shift(ppm)
A *1 4.46 B *1 4.43 C *1 3.932 D *1 3.896 E 3.20 F 2.91 G 2.824 J 2.642 K 2.02 L 1.805 M 1.529 N 1.438 ASSIGNED BY C-H COSY
Hz ppm Int.1786.99 4.472 257 1784.06 4.465 324 1783.20 4.462 346 1782.10 4.460 351 1781.01 4.457 376 1780.27 4.455 374 1779.17 4.452 346 1778.08 4.450 317 1774.78 4.441 300 1771.73 4.434 356 1771.00 4.432 384 1769.78 4.429 384 1768.68 4.426 410 1767.94 4.424 417 1766.97 4.422 385 1765.75 4.419 353 1579.96 3.954 275 1578.25 3.950 283 1573.73 3.938 310 1572.14 3.934 494 1567.75 3.923 514 1566.04 3.919 538 1561.40 3.907 533 1559.94 3.904 493 1555.54 3.893 273 1553.71 3.888 291 1549.07 3.877 267 1287.48 3.222 115 1284.91 3.216 250 1282.35 3.209 412 1280.64 3.205 426 1278.32 3.199 549 1275.88 3.193 502 1274.54 3.190 382 1273.32 3.187 355 1272.09 3.184 334 1270.39 3.179 171 1269.41 3.177 185 1173.71 2.937 149 1169.31 2.926 224 1165.53 2.917 296 1165.28 2.916 296 1161.99 2.908 319 1156.37 2.894 231 1151.61 2.882 158 1146.97 2.870 97 1134.16 2.838 405 1133.54 2.837 453 1132.57 2.834 607 1129.39 2.826 798 1128.54 2.824 961 1127.81 2.822 841 1125.12 2.816 465 1124.51 2.814 499 1123.54 2.812 644 1061.16 2.656 350 1058.96 2.650 923 1056.40 2.644 1000 1054.08 2.638 845 1051.51 2.632 718 819.46 2.051 141 814.09 2.038 201 812.99 2.035 196 811.16 2.030 210 810.79 2.029 210 808.84 2.024 215 806.52 2.019 244 802.12 2.008 237 801.76 2.007 237 798.58 1.999 203 798.22 1.998 203 790.41 1.978 92 734.13 1.837 179 730.10 1.827 249 726.20 1.818 267 721.44 1.806 272 717.04 1.795 228 712.65 1.784 202 708.86 1.774 160 625.37 1.565 131 621.70 1.556 183 617.80 1.546 218 613.89 1.537 235 613.40 1.535 235 611.82 1.531 237 607.67 1.521 253 607.42 1.520 253 603.88 1.512 212 599.49 1.501 162 595.21 1.490 107 585.82 1.466 183 585.57 1.466 183 583.98 1.462 175 577.88 1.446 267 573.73 1.436 263 567.87 1.421 216 565.55 1.416 198
in CDCl3
liquid film
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