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MassMS-IW-6293 1-(3-chloropropyl)piperidine hydrochloride C8H16ClN HCl (Mass of molecular ion: 161)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
27.0 1.0 28.0 1.4 30.0 1.2 36.0 9.7 38.0 3.2 39.0 1.3 41.0 5.5 42.0 5.6 43.0 1.9 44.0 2.8 55.0 5.7 56.0 1.4 69.0 2.4 70.0 3.5 84.0 1.4 96.0 1.3 98.0 100.0 99.0 7.2 160.0 3.7 161.0 7.3 162.0 1.9 163.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H16 Cl N 0.046 g : 0.5 ml CDCl3 1-(3-chloropropyl)piperidine hydrochloride 
Assign. Shift(ppm)
A 3.697 B 3.544 C 3.188 D 2.843 E 2.467 F 2.24 G 1.895 J 1.50
Hz ppm Int.1483.52 3.713 814 1477.54 3.698 1000 1474.49 3.690 141 1471.56 3.683 813 1420.53 3.555 304 1408.94 3.526 311 1280.40 3.204 247 1275.15 3.191 300 1274.54 3.190 300 1268.43 3.174 251 1152.47 2.884 115 1142.33 2.859 218 1132.81 2.835 212 1121.70 2.807 101 998.66 2.499 197 992.55 2.484 314 990.60 2.479 218 989.26 2.476 207 986.69 2.469 337 984.50 2.464 296 982.42 2.459 343 976.07 2.443 268 970.34 2.428 154 917.60 2.297 88 914.06 2.288 80 905.03 2.265 208 902.95 2.260 199 893.43 2.236 198 890.26 2.228 224 881.10 2.205 87 877.69 2.197 101 874.51 2.189 67 762.82 1.909 495 751.71 1.881 436 616.58 1.543 61 613.28 1.535 54 605.22 1.515 113 603.76 1.511 119 600.71 1.504 113 594.36 1.488 92 591.19 1.480 107
in CDCl3
KBr disc
nujol mull
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