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网站主页CAS数据库列表 5465-63-4更多图谱2-溴苄胺盐酸盐(5465-63-4)核磁图(1HNMR)

2-溴苄胺盐酸盐

产品名称 2-溴苄胺盐酸盐

CAS号5465-63-4

分子式C7H9BrClN

分子量222.51

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  • Mass

    MS-IW-9291          
    2-bromobenzylamine hydrochloride
    C7H8BrN HCl         (Mass of molecular ion:    185)
    

       Source Temperature: 170 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       1.5
          27.0       2.1
          28.0      31.5
          29.0       9.7
          30.0      60.1
          35.0       4.9
          36.0      45.7
          37.0       2.6
          38.0      16.3
          39.0       5.3
          49.0       1.1
          50.0      11.5
          51.0      16.5
          51.5       2.5
          52.0       5.6
          52.5      20.0
          53.0       7.1
          61.0       1.0
          62.0       2.4
          63.0       4.9
          64.0       1.3
          74.0       4.2
          75.0       6.7
          76.0       6.6
          77.0      42.6
          78.0      16.0
          79.0      19.4
          80.0       1.8
          89.0       6.9
          90.0       7.3
          91.0       1.7
         102.0       2.4
         103.0       1.4
         104.0       9.2
         105.0       2.7
         106.0     100.0
         107.0       8.3
         156.0       3.4
         157.0       5.2
         158.0       3.5
         159.0       4.8
         169.0       6.1
         171.0       5.7
         184.0      30.7
         185.0      14.1
         186.0      30.2
         187.0      13.3
         188.0       1.1
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C7 H8 Br N 0.041 g : 0.5 ml DMSO-d6
    2-bromobenzylamine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.81 B 7.702 C 7.695 D 7.470 E 7.340 F 4.107

         Hz     ppm     Int.
    

       3522.49   8.814     48
       3083.65   7.716    176
       3081.97   7.712    199
       3080.44   7.708    262
       3079.22   7.705    269
       3075.87   7.697    216
       3074.34   7.693    226
       3072.36   7.688    290
       3071.14   7.685    289
       2993.77   7.491    114
       2992.71   7.489    123
       2986.30   7.473    230
       2985.08   7.470    240
       2978.67   7.454    133
       2977.45   7.451    134
       2941.28   7.360    128
       2939.76   7.356    137
       2933.50   7.341    186
       2931.98   7.337    186
       2925.87   7.322     93
       2924.35   7.318     93
       1641.54   4.108   1000
    

in DMSO-d6



KBr disc



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