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网站主页CAS数据库列表 544-16-1更多图谱亚硝酸丁酯(544-16-1)质谱(MS)

亚硝酸丁酯

产品名称 亚硝酸丁酯

CAS号544-16-1

分子式C4H9NO2

分子量103.12

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  • Mass

    MS-KW-0243          
    butyl nitrite
    C4H9NO2             (Mass of molecular ion:    103)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       3.0
          18.0       2.8
          19.0       1.0
          26.0       4.0
          27.0      55.1
          28.0      13.8
          29.0      35.0
          30.0      63.7
          31.0      26.3
          33.0       2.0
          37.0       1.1
          38.0       2.2
          39.0      18.2
          40.0       3.3
          41.0      95.7
          42.0      14.4
          43.0     100.0
          44.0      13.5
          45.0       2.8
          53.0       1.5
          54.0       1.2
          55.0       8.6
          56.0      33.1
          57.0      34.2
          58.0       1.6
          60.0      57.4
          61.0       1.1
          71.0       8.8
          72.0       5.9
          73.0       2.5
          89.0       3.3
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C4 H9 N O2 0.04 ml : 0.5 ml CDCl3
    butyl nitrite
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.697 B 1.68 C 1.40 D 0.956

         Hz     ppm     Int.
    

        427.63   4.775    318
        421.19   4.703    751
        414.69   4.631    434
        169.69   1.895     50
        168.06   1.877     51
        167.69   1.873     45
        163.38   1.825     98
        162.75   1.818     93
        161.63   1.805    139
        161.25   1.801    141
        159.38   1.780     92
        158.75   1.773     75
        157.81   1.763     97
        156.75   1.751     97
        154.75   1.728    291
        153.75   1.717    202
        152.94   1.708    186
        152.13   1.699    155
        151.00   1.687     97
        150.50   1.681     61
        148.19   1.655    279
        147.31   1.645    232
        146.38   1.635    181
        145.56   1.626    116
        143.56   1.603    178
        142.56   1.592    141
        142.00   1.586    173
        141.50   1.580    153
        140.69   1.571    126
        140.06   1.564    104
        138.13   1.543    166
        137.38   1.534    171
        136.94   1.530    203
        136.19   1.521    227
        135.69   1.516    136
        134.31   1.500     86
        133.94   1.496     82
        133.38   1.490     99
        132.00   1.474    182
        131.00   1.463    233
        130.00   1.452    192
        128.69   1.437    289
        127.06   1.419     96
        126.50   1.413    101
        126.06   1.408     90
        125.06   1.397    148
        124.56   1.391    163
        124.06   1.386    170
        121.94   1.362    310
        121.06   1.352    145
        119.44   1.334     91
        118.25   1.321     93
        117.19   1.309     40
        116.56   1.302     42
        115.38   1.289    236
        114.19   1.276    139
        112.75   1.259     45
        108.94   1.217    118
        102.13   1.141     77
        101.56   1.134     57
         94.31   1.054     49
         93.13   1.040    393
         91.94   1.027    641
         91.25   1.019    630
         90.44   1.010    308
         88.63   0.990     88
         88.00   0.983     81
         87.56   0.978     72
         85.44   0.954   1000
         85.06   0.950    844
         84.00   0.938    563
         82.31   0.920    205
         80.31   0.897    125
         79.81   0.892    167
         79.44   0.888    173
         79.06   0.883    203
         78.00   0.871    302
         76.13   0.851    190
    


  • 1H NMR 399.65 MHz
    C4H9NO2 0.05 ml : 0.5 ml CDCl3
    butyl nitrite
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.706 B 1.724 C 1.414 D 0.958

         Hz     ppm     Int.
    

       1881.11   4.706    108
        703.01   1.759     78
        696.42   1.742    184
        693.36   1.735     69
        689.09   1.724    220
        681.16   1.704    193
        674.57   1.688     90
        583.87   1.461     63
        576.54   1.443    179
        570.68   1.428    105
        568.97   1.424    248
        563.36   1.410    105
        561.28   1.404    263
        555.91   1.391     53
        553.96   1.386    177
        546.51   1.368     60
        463.63   1.160     14
        456.06   1.141     24
        448.49   1.122     13
        389.78   0.975    581
        382.33   0.957   1000
        375.01   0.939    495
        318.97   0.798     12
    

in CDCl3



liquid film