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网站主页CAS数据库列表 542-69-8更多图谱1-碘丁烷(542-69-8)红外图谱(IR2)

1-碘丁烷

产品名称 1-碘丁烷

CAS号542-69-8

分子式C4H9I

分子量184.02

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  • Mass

    MS-NW-8348          
    1-iodobutane
    C4H9I               (Mass of molecular ion:    184)
    

       Source Temperature: 250 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          26.0       2.0
          27.0      18.2
          28.0       6.8
          29.0      61.7
          30.0       1.4
          39.0       8.7
          41.0      50.4
          42.0       2.2
          43.0       1.6
          53.0       1.0
          55.0       4.6
          56.0       1.4
          57.0     100.0
          58.0       4.6
         127.0       3.7
         128.0       1.6
         155.0       2.1
         184.0      15.1
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C4 H9 I 0.04 ml : 0.5 ml CDCl3
    1-iodobutane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.195 B 1.80 C 1.42 D 0.93

         Hz     ppm     Int.
    

        293.56   3.278    343
        286.63   3.201   1000
        279.81   3.125    484
        177.13   1.978     53
        176.19   1.968     58
        170.44   1.904    150
        170.00   1.899    140
        169.13   1.889     86
        168.75   1.885     89
        167.38   1.869     63
        163.00   1.821    235
        161.94   1.809    143
        160.44   1.792    102
        158.63   1.772     42
        157.63   1.761     46
        156.19   1.744    205
        155.38   1.735    210
        153.81   1.718     56
        153.56   1.715     56
        153.19   1.711     58
        149.06   1.665     90
        148.44   1.658     75
        145.38   1.624     76
        139.38   1.557     90
        138.56   1.548     96
        137.69   1.538    144
        136.38   1.523     79
        135.38   1.512     37
        135.00   1.508     33
        134.06   1.497     48
        132.81   1.483    104
        132.13   1.476    122
        131.19   1.465    173
        130.06   1.453    176
        128.81   1.439     66
        127.00   1.419     55
        125.56   1.402    141
        123.31   1.377    194
        120.31   1.344     39
        119.25   1.332     61
        116.69   1.303    150
        116.00   1.296    121
        115.13   1.286     39
        112.81   1.260     43
        110.38   1.233     74
         90.31   1.009    292
         89.38   0.998    488
         85.63   0.957     37
         82.69   0.924    877
         79.00   0.883     51
         76.69   0.857    117
         76.25   0.852    119
         75.31   0.841    217
         73.63   0.823    105
    

in CDCl3



CCl4 solution



liquid film





REACTION WITH NA AT 77K