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网站主页CAS数据库列表 5402-73-3更多图谱2,5-二氯苄磺酸氯(5402-73-3)红外图谱(IR1)

2,5-二氯苄磺酸氯

产品名称 2,5-二氯苄磺酸氯

CAS号5402-73-3

分子式C6H3Cl3O2S

分子量245.51

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  • Mass

    MS-IW-5084          
    2,5-dichlorobenzenesulfonyl chloride
    C6H3Cl3O2S          (Mass of molecular ion:    244)
    

       Source Temperature: 110 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          36.0       1.2
          37.0       2.6
          38.0       1.7
          45.0       1.0
          48.0       2.3
          49.0       1.9
          50.0       7.6
          51.0       1.2
          54.5       2.8
          55.0       2.3
          55.5       1.0
          61.0       2.5
          62.0       2.2
          63.0       2.7
          64.0       2.4
          69.0       2.4
          72.0       1.9
          72.5       1.1
          73.0       7.1
          74.0      26.1
          75.0      20.3
          76.0       1.3
          79.0       1.2
          83.0       1.0
          84.0       7.5
          85.0       5.2
          86.0       2.6
          87.0       1.6
          90.0       1.2
          91.0       1.3
          95.0       1.1
          97.0       1.0
         104.5       3.3
         105.5       2.2
         107.0       1.1
         108.0       1.9
         109.0      42.2
         110.0       9.3
         111.0      14.4
         112.0       2.9
         119.0       1.0
         133.0       3.2
         135.0       2.0
         142.0       1.1
         144.0       1.1
         145.0     100.0
         146.0       8.0
         147.0      65.0
         148.0       4.9
         149.0      10.3
         161.0       3.6
         163.0       2.3
         165.0       1.5
         180.0       6.3
         182.0       5.9
         184.0       1.9
         193.0       1.2
         209.0      86.4
         210.0       6.5
         211.0      59.3
         212.0       4.1
         213.0      11.2
         244.0      26.0
         245.0       2.1
         246.0      26.2
         247.0       2.0
         248.0       9.1
         250.0       1.3
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H3 Cl3 O2 S 0.039 g : 0.5 ml CDCl3
    2,5-dichlorobenzenesulfonyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.130 B 7.63 C 7.59 CALCULATED BY LAOCN PROGRUM.

         Hz     ppm     Int.
    

        729.75   8.149    331
        728.75   8.138    319
        727.94   8.128    436
        726.94   8.117    407
        691.25   7.719     56
        682.69   7.623    651
        681.63   7.611    673
        680.63   7.600   1000
        673.06   7.516     40
    

in CDCl3



KBr disc



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