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MassMS-IW-0034 2-bromo-1-indanol C9H9BrO (Mass of molecular ion: 212)
Source Temperature: 130 °C Sample Temperature: 100 °C Direct, 75 eV
27.0 1.2 39.0 1.5 50.0 1.7 51.0 6.4 52.0 1.8 55.0 13.3 57.5 1.4 63.0 1.9 65.0 2.4 65.5 1.9 66.0 5.4 76.0 1.1 77.0 8.2 78.0 1.8 79.0 5.8 89.0 1.3 91.0 4.1 102.0 1.3 103.0 7.0 104.0 2.7 105.0 11.2 115.0 11.0 116.0 4.7 131.0 4.8 132.0 8.0 133.0 100.0 134.0 9.9 211.0 1.3 212.0 17.1 213.0 3.0 214.0 16.8 215.0 1.7
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C9 H9 Br O 0.037 g : 0.5 ml DMSO-d6 2-bromo-1-indanol 
Assign. Shift(ppm)
A 7.35 B 7.28 to 7.23 C 5.99 D 5.092 E 4.323 F 3.557 G 3.102 J(C,D)=6.6HZ J(F,E)=7.1HZ J(F,G)=-16.4HZ J(G,E)=6.8HZ
Hz ppm Int.2943.24 7.365 203 2942.38 7.363 202 2939.70 7.356 145 2937.87 7.352 322 2934.94 7.344 298 2930.91 7.334 60 2913.21 7.290 55 2908.33 7.278 283 2906.86 7.274 302 2902.83 7.264 1000 2899.66 7.256 721 2897.95 7.252 771 2893.55 7.241 331 2890.14 7.232 86 2888.18 7.227 101 2887.45 7.225 106 2397.34 5.999 905 2390.75 5.983 937 2041.02 5.108 246 2035.16 5.093 413 2028.93 5.077 247 1737.55 4.348 203 1732.06 4.334 249 1730.71 4.331 469 1725.10 4.317 463 1723.75 4.314 262 1718.26 4.300 212 1434.08 3.589 233 1427.12 3.571 227 1417.72 3.548 276 1410.77 3.531 260 1250.73 3.130 247 1243.90 3.113 241 1234.50 3.089 206 1227.66 3.072 202
in DMSO-d6
KBr disc
nujol mull
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