N-(4-溴丁基)邻苯二甲酰亚胺

产品名称 N-(4-溴丁基)邻苯二甲酰亚胺

CAS号5394-18-3

分子式C12H12BrNO2

分子量282.13

¹³CNMR

Mass

MS-NW-8793          
N-(4-bromobutyl)phthalimide
C12H12BrNO2         (Mass of molecular ion:    281)

   Source Temperature: 170 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       1.0
      27.0       1.8
      28.0       1.0
      39.0       1.4
      41.0       1.8
      50.0       4.0
      51.0       2.3
      53.0       1.0
      55.0       1.6
      74.0       1.2
      75.0       2.7
      76.0      10.0
      77.0       9.2
     102.0       2.2
     103.0       1.2
     104.0       8.3
     105.0       6.6
     130.0       7.7
     132.0       1.2
     133.0       4.9
     147.0       1.2
     148.0       3.4
     160.0     100.0
     161.0      10.7
     174.0       4.9
     175.0       1.1
     188.0       2.0
     201.0      12.0
     202.0      47.3
     203.0       6.4
     281.0       3.7
     283.0       3.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₁₂ Br N O₂	0.036 g : 0.5 ml CDCl₃
N-(4-bromobutyl)phthalimide

    Assign.     Shift(ppm)

      A             7.849
      B             7.730
      C             3.731
      D             3.451
      E             1.90
      F             1.86

     Hz     ppm     Int.

   3147.22   7.875     36
   3145.75   7.872     53
   3141.97   7.862    719
   3138.92   7.855    715
   3136.35   7.848    556
   3133.42   7.841    977
   3130.25   7.833     60
   3129.52   7.831    116
   3128.30   7.828    103
   3098.39   7.753     81
   3097.17   7.750    102
   3095.95   7.747     37
   3093.38   7.741    901
   3090.33   7.733    559
   3087.89   7.727    684
   3084.84   7.719    713
   3081.05   7.710     85
   3079.59   7.706     55
   1497.80   3.748    459
   1490.97   3.731    878
   1484.25   3.714    381
   1385.99   3.469    398
   1379.64   3.453   1000
   1373.17   3.436    522
    780.52   1.954     42
    778.44   1.948     44
    773.93   1.937    100
    771.61   1.931    129
    768.55   1.924    128
    766.36   1.918    140
    765.14   1.915    237
    762.57   1.909    181
    761.96   1.907    164
    758.91   1.899    301
    757.69   1.896    278
    755.37   1.891    230
    754.39   1.888    231
    753.30   1.885    224
    752.20   1.883    234
    749.76   1.877    265
    748.41   1.873    283
    744.87   1.864    189
    742.92   1.859    199
    742.07   1.857    219
    741.09   1.855    166
    738.53   1.848    119
    735.60   1.841    127
    733.15   1.835    122
    728.64   1.824     49
    726.44   1.818     47

in CDCl3

KBr disc

nujol mull

4880 A,200 M,powder

更多供应商

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