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2-BROMO-N,N-DIETHYLETHYLAMINE HYDROBROMIDE

产品名称 2-BROMO-N,N-DIETHYLETHYLAMINE HYDROBROMIDE

CAS号5392-81-4

分子式C6H14BrN

分子量180.09

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  • Mass

    MS-NW-6609          
    2-bromotriethylamine hydrobromide
    C6H14BrN HBr        (Mass of molecular ion:    179)
    

       Source Temperature: 150 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          15.0       3.5
          17.0       1.0
          18.0       4.3
          26.0       2.4
          27.0      20.5
          28.0      14.8
          29.0      17.4
          30.0      16.1
          39.0       1.0
          40.0       1.0
          41.0       4.3
          42.0      18.3
          43.0       3.1
          44.0      41.2
          45.0       1.0
          54.0       2.3
          55.0       1.9
          56.0      12.6
          57.0       4.7
          58.0      14.1
          70.0       4.5
          71.0       3.6
          72.0      19.0
          79.0       9.8
          80.0      29.7
          81.0       9.9
          82.0      28.3
          84.0       2.4
          85.0       1.2
          86.0     100.0
          87.0       6.2
          98.0       1.0
          99.0       1.2
         100.0      65.0
         101.0       5.0
         107.0       7.9
         108.0       1.7
         109.0       6.7
         110.0       1.6
         122.0       1.0
         136.0       5.0
         138.0       5.0
         164.0      11.8
         166.0      11.0
         178.0       1.1
         179.0      10.9
         180.0       1.9
         181.0      10.5
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C6 H14 Br N 0.039 g : 0.5 ml DMSO-d6
    2-bromotriethylamine hydrobromide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.77 B 3.853 C 3.54 D 3.22 E 1.231

         Hz     ppm     Int.
    

       1547.70   3.873    131
       1543.88   3.864     32
       1540.68   3.856    226
       1539.46   3.853    138
       1536.10   3.844     33
       1532.75   3.836    164
       1423.19   3.562     72
       1418.15   3.549     85
       1415.41   3.542    108
       1410.37   3.530    105
       1408.39   3.525     68
       1403.20   3.512     55
       1303.41   3.262     31
       1302.19   3.259     37
       1300.96   3.256     35
       1294.86   3.240    103
       1290.28   3.229    103
       1287.38   3.222    129
       1286.77   3.220    126
       1282.96   3.211    119
       1281.74   3.208    119
       1279.30   3.202    110
       1274.41   3.189    104
       1268.31   3.174     42
       1267.24   3.171     48
        499.27   1.250    464
        492.10   1.232   1000
        484.77   1.213    443
    

KBr disc



nujol mull



4880 A,200 M,powder



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