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网站主页CAS数据库列表 537-91-7更多图谱3,3'-二硝基二苯二硫醚(537-91-7)核磁图(13CNMR)

3,3'-二硝基二苯二硫醚

产品名称 3,3'-二硝基二苯二硫醚

CAS号537-91-7

分子式C12H8N2O4S2

分子量308.33

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  • Mass

    MS-NW-6861          
    bis(m-nitrophenyl) disulfide
    C12H8N2O4S2         (Mass of molecular ion:    308)
    

       Source Temperature: 180 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          18.0       3.6
          28.0       1.0
          30.0       1.5
          38.0       1.3
          39.0       2.6
          45.0       3.8
          50.0       2.6
          51.0       1.3
          58.0       5.2
          62.0       1.3
          63.0       6.7
          64.0       2.2
          65.0       1.3
          69.0      17.3
          70.0       2.0
          71.0       1.5
          74.0       1.0
          75.0       1.7
          76.0       2.4
          81.0       1.2
          82.0       8.2
          92.0       1.1
          95.0       1.6
          96.0       7.1
         107.0       1.6
         108.0      35.9
         109.0       6.0
         110.0       2.1
         124.0       2.5
         138.0       2.3
         139.0       1.1
         140.0       4.0
         154.0       9.6
         155.0       4.4
         156.0       1.0
         168.0       4.2
         170.0       3.0
         171.0       7.5
         172.0       1.7
         184.0       1.1
         199.0       4.1
         200.0       1.6
         203.0       5.0
         204.0       4.3
         205.0       1.1
         215.0       1.2
         230.0       1.1
         308.0     100.0
         309.0      15.7
         310.0      11.3
         311.0       1.6
    

90 MHz in CDCl3

in CDCl3


  • 1H NMR 89.56 MHz
    C12 H8 N2 O4 S2 0.040 g : 0.5 ml CDCl3
    bis(m-nitrophenyl) disulfide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.364 B 8.099 C 7.804 D 7.537

         Hz     ppm     Int.
    

        751.50   8.392    462
        751.13   8.387    438
        749.38   8.368   1000
        747.50   8.347    686
        747.06   8.342    567
        731.50   8.168    375
        730.31   8.155    458
        729.31   8.144    334
        728.13   8.131    339
        723.50   8.079    486
        722.31   8.066    574
        721.38   8.055    457
        720.19   8.042    475
        705.50   7.878    321
        704.31   7.865    428
        703.63   7.857    321
        702.44   7.844    352
        697.63   7.790    662
        696.44   7.777    679
        695.75   7.769    682
        694.56   7.756    541
        681.50   7.610    830
        681.00   7.604    751
        673.56   7.521    976
        673.13   7.516    910
        665.63   7.433    358
        665.19   7.428    334
    



in CDCl3



KBr disc



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