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网站主页CAS数据库列表 537-45-1更多图谱2,6-二溴喹柄-4-氯亚胺(537-45-1)核磁图(13CNMR)

2,6-二溴喹柄-4-氯亚胺

产品名称 2,6-二溴喹柄-4-氯亚胺

CAS号537-45-1

分子式C6H2Br2ClNO

分子量299.35

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  • Mass

    MS-NW-0396          
    2,6-dibromo-N-chloro-p-benzoquinone monoimine
    C6H2Br2ClNO         (Mass of molecular ion:    297)
    

       Source Temperature: 130 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       2.5
          25.0       4.5
          26.0       1.3
          28.0       1.6
          35.0       1.0
          36.0       3.9
          37.0       6.2
          38.0       1.8
          48.0       1.5
          49.0       6.8
          50.0      11.2
          51.0      25.4
          52.0      11.6
          53.0      51.4
          54.0       1.8
          55.5       1.5
          60.0       1.8
          61.0       4.8
          62.0       3.5
          74.0       1.5
          75.0      10.6
          76.0      23.4
          77.0       2.2
          78.0       2.2
          79.0       2.9
          80.0       1.0
          81.0       2.6
          86.0       6.0
          88.0       2.0
          95.0       1.4
          96.0       1.8
         104.0       9.4
         105.0       1.5
         106.0       9.9
         107.0       1.3
         110.0       4.1
         111.0       3.8
         112.0       1.7
         113.0       1.3
         114.0       9.0
         116.0       2.9
         128.0       1.1
         129.0       4.0
         130.0      25.7
         131.0       6.1
         132.0      24.7
         133.0       2.1
         141.0       1.5
         154.0      12.9
         155.0       8.4
         156.0      14.9
         157.0      10.4
         158.0      15.5
         159.0       2.9
         160.0      13.2
         163.0       1.2
         165.0       4.3
         167.0      12.6
         169.0      12.5
         171.0       2.9
         183.0       3.3
         184.0       7.8
         185.0       4.2
         186.0       7.7
         190.0      11.5
         192.0      14.8
         194.0       3.8
         210.0       1.6
         218.0      16.2
         219.0       1.6
         220.0      21.5
         221.0       1.9
         222.0       5.4
         234.0       4.9
         236.0      11.3
         238.0       8.5
         240.0       2.0
         262.0       1.1
         263.0       9.7
         264.0       3.0
         265.0      19.4
         266.0       2.8
         267.0       9.9
         269.0       1.5
         271.0       2.7
         273.0       2.0
         297.0      45.0
         298.0       3.2
         299.0     100.0
         300.0       6.8
         301.0      68.5
         302.0       4.9
         303.0      13.4
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H2 Br2 Cl N O 0.042 g : 0.5 ml CDCl3
    2,6-dibromo-N-chloro-p-benzoquinone monoimine
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 8.268 B *1 7.774

         Hz     ppm     Int.
    

       3308.11   8.278     33
       3305.54   8.272   1000
       3302.98   8.265    990
       3300.42   8.259     24
       3108.40   7.778    984
       3105.83   7.772    967
       3103.52   7.766     41
    


  • 1H NMR 89.56 MHz
    C6 H2 Br2 Cl N O saturated in CDCl3
    2,6-dibromo-N-chloro-p-benzoquinone monoimine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.258 B 7.763

         Hz     ppm     Int.
    

        741.00   8.274    895
        738.44   8.246   1000
        696.56   7.778    994
        695.50   7.766     38
        694.00   7.749    892
    

in CDCl3



CCl4 solution



KBr disc



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