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MassMS-IW-0553 6-chloro-3-pyridinamine C5H5ClN2 (Mass of molecular ion: 128)
Source Temperature: 250 °C Sample Temperature: 160 °C Reservoir, 75 eV
18.0 2.0 28.0 3.5 36.0 1.0 37.0 2.9 38.0 4.7 39.0 9.6 40.0 3.8 41.0 8.1 42.0 2.0 49.0 1.1 50.0 1.3 51.0 1.3 52.0 3.0 63.0 1.0 64.0 3.6 65.0 3.5 66.0 31.0 67.0 4.0 72.0 1.0 73.0 5.5 74.0 1.7 75.0 2.7 76.0 1.2 92.0 1.9 93.0 40.2 94.0 2.6 100.0 2.8 101.0 7.6 102.0 1.4 103.0 2.5 127.0 1.3 128.0 100.0 129.0 7.7 130.0 32.4 131.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C5 H5 Cl N2 0.028 g : 0.5 ml CDCl3 6-chloro-3-pyridinamine 
Assign. Shift(ppm)
A 7.838 B 7.074 C 6.967 D 3.84
Hz ppm Int.3134.16 7.843 755 3131.23 7.835 765 2832.28 7.087 698 2823.73 7.066 1000 2789.55 6.980 626 2786.50 6.973 621 2781.01 6.959 441 2778.08 6.952 430 1533.20 3.837 264
in CDCl3
KBr disc
nujol mull
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