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3-甲基-2-硝基苯甲醚

产品名称 3-甲基-2-硝基苯甲醚

CAS号5345-42-6

分子式C8H9NO3

分子量167.16

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  • Mass

    MS-IW-8126          
    3-methyl-2-nitroanisole
    C8H9NO3             (Mass of molecular ion:    167)
    

       Source Temperature: 200 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.9
          27.0       2.6
          28.0       2.7
          29.0       1.1
          30.0       2.6
          37.0       1.2
          38.0       3.0
          39.0      14.8
          40.0       2.2
          41.0       4.0
          42.0       1.9
          43.0       1.3
          50.0       7.8
          51.0      19.5
          52.0      14.4
          53.0       9.3
          54.0       1.0
          55.0       1.8
          59.0       4.9
          61.0       1.3
          62.0       3.7
          63.0      10.6
          64.0       4.5
          65.0      40.3
          66.0      10.3
          67.0       4.3
          68.0       1.0
          74.0       2.2
          75.0       2.1
          76.0       3.3
          77.0      28.8
          78.0      26.9
          79.0       8.4
          80.0       4.0
          81.0       4.5
          89.0       7.3
          90.0      10.7
          91.0      60.5
          92.0      14.0
          93.0       7.9
          94.0      16.1
          95.0      27.4
          96.0       2.2
         104.0       1.3
         105.0      19.5
         106.0      17.9
         107.0       6.0
         108.0       5.3
         109.0       4.3
         118.0       1.5
         119.0       1.4
         120.0       7.8
         121.0       2.0
         122.0       7.7
         123.0       1.4
         135.0       8.0
         136.0       2.8
         137.0       1.6
         150.0      97.5
         151.0       9.4
         152.0       1.1
         167.0     100.0
         168.0       9.6
         169.0       1.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H9 N O3 0.043 g : 0.5 ml CDCl3
    3-methyl-2-nitroanisole
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.284 B 6.86 C 3.868 D 2.294

         Hz     ppm     Int.
    

        661.88   7.391     48
        654.50   7.308     60
        653.13   7.293     62
        645.88   7.212     90
        618.31   6.904    101
        616.94   6.889    101
        616.25   6.881     93
        609.56   6.807     89
        608.94   6.800     80
        608.31   6.793     57
        607.75   6.786     41
        346.50   3.869   1000
        344.50   3.847     47
        205.50   2.295    555
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder