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邻氨基苯甲醇

CAS号5344-90-1

分子式C7H9NO

分子量123.15

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  • Mass

    MS-NW-6136          
    o-aminobenzyl alcohol
    C7H9NO              (Mass of molecular ion:    123)
    

       Source Temperature: 250 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          17.0       2.0
          18.0       9.2
          26.0       1.1
          27.0       3.9
          28.0       5.5
          29.0       2.3
          30.0       2.5
          31.0       1.4
          37.0       2.1
          38.0       4.5
          39.0      13.3
          40.0       2.3
          41.0       4.9
          42.0       1.9
          46.5       1.3
          50.0       5.8
          51.0      13.2
          52.0       9.8
          53.0       3.5
          54.0       2.5
          61.0       2.8
          62.0       2.3
          63.0       4.5
          64.0       2.6
          65.0      12.0
          66.0       6.9
          67.0       3.1
          74.0       1.7
          75.0       1.7
          76.0       3.7
          77.0      33.6
          78.0      47.9
          79.0       9.2
          80.0       1.7
          91.0       2.0
          92.0       6.7
          93.0      11.7
          94.0      17.0
          95.0       1.5
         103.0       1.2
         104.0      72.6
         105.0      83.7
         106.0      27.6
         107.0       3.8
         120.0       2.6
         121.0       1.5
         122.0       6.7
         123.0     100.0
         124.0       8.4
         198.0       1.3
         210.0       1.7
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H9 N O 0.043 g : 0.5 ml CDCl3
    o-aminobenzyl alcohol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.08 B 7.00 C 6.68 D 6.65 E 4.537 F 3.52 J(A,B)=1.7HZ. J(C,D)=1.3HZ.

         Hz     ppm     Int.
    

        644.88   7.201     61
        643.06   7.181     74
        637.31   7.117    136
        635.63   7.098    160
        633.75   7.077     48
        629.94   7.034    189
        628.25   7.015    187
        623.69   6.964    173
        622.50   6.951    153
        606.44   6.772    126
        605.13   6.757    195
        597.94   6.677    439
        591.75   6.608     70
        590.38   6.593    216
        406.38   4.538   1000
        314.81   3.516    490
    

in CDCl3



KBr disc



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