-
MassMS-NW-6240 benzil monohydrazone C14H12N2O (Mass of molecular ion: 224)
Source Temperature: 160 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 3.0 27.0 1.0 28.0 1.9 39.0 2.2 50.0 3.9 51.0 14.0 52.0 1.3 63.0 2.1 65.0 1.2 74.0 1.2 75.0 1.5 76.0 4.5 77.0 65.9 78.0 4.8 89.0 1.2 91.0 1.5 92.0 1.3 103.0 4.3 104.0 2.1 105.0 32.3 106.0 2.9 119.0 100.0 120.0 8.7 165.0 3.5 166.0 1.1 178.0 1.6 196.0 3.4 223.0 6.0 224.0 33.9 225.0 5.7
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C14 H12 N2 O 0.039 g : 0.5 ml DMSO-d6 benzil monohydrazone 
Assign. Shift(ppm)
A 8.00 B 7.772 C 7.51 D 7.50 E 7.44 F 7.42 G 7.273
Hz ppm Int.3189.70 7.982 292 3110.96 7.785 603 3109.59 7.781 788 3108.06 7.777 384 3104.86 7.769 253 3102.72 7.764 999 3101.20 7.760 754 3009.03 7.530 239 3007.97 7.527 405 3006.59 7.524 214 3005.37 7.521 216 3004.00 7.517 165 3002.47 7.513 294 3000.79 7.509 1000 2999.57 7.506 574 2998.20 7.503 558 2995.61 7.496 251 2994.69 7.494 343 2993.32 7.490 715 2992.55 7.488 659 2990.88 7.484 515 2989.35 7.480 264 2978.67 7.454 725 2977.45 7.451 340 2975.62 7.446 260 2974.24 7.443 469 2972.87 7.439 720 2971.34 7.435 935 2969.21 7.430 316 2966.77 7.424 506 2964.32 7.418 501 2962.95 7.414 261 2960.82 7.409 131 2959.44 7.406 191 2911.53 7.286 763 2910.00 7.282 942 2908.02 7.277 234 2904.51 7.268 369 2903.14 7.265 781 2901.92 7.262 563
in DMSO-d6
KBr disc
nujol mull
4880 A,200 M,powder
更多供应商
