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网站主页CAS数据库列表 5339-26-4更多图谱4-硝基苯乙基溴(5339-26-4)Raman光谱

4-硝基苯乙基溴

产品名称 4-硝基苯乙基溴

CAS号5339-26-4

分子式C8H8BrNO2

分子量230.06

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  • Mass

    MS-IW-6133          
    p-nitrophenethyl bromide
    C8H8BrNO2           (Mass of molecular ion:    229)
    

       Source Temperature: 130 °C
       Sample Temperature:  90 °C
       Direct, 75 eV
    

          27.0       2.9
          30.0       8.4
          38.0       1.6
          39.0       6.0
          50.0       9.9
          51.0      13.7
          52.0       4.1
          53.0       1.7
          62.0       2.8
          63.0       9.1
          64.0       2.5
          65.0       4.1
          74.0       4.9
          75.0       5.2
          76.0       6.2
          77.0      34.1
          78.0      31.1
          79.0       2.2
          89.0       8.8
          90.0       9.1
          91.0      12.1
          92.0       7.6
          93.0       1.1
         101.0       1.6
         102.0       8.7
         103.0      32.7
         104.0      39.7
         105.0       3.8
         106.0      18.1
         107.0       1.6
         119.0       4.5
         120.0      13.8
         121.0       1.4
         136.0      50.6
         137.0       4.1
         149.0       9.0
         150.0     100.0
         151.0       9.5
         183.0       6.5
         185.0       6.3
         213.0       1.7
         215.0       1.7
         229.0      98.8
         230.0       9.4
         231.0      97.1
         232.0       9.1
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H8 Br N O2 0.041 g : 0.5 ml CDCl3
    p-nitrophenethyl bromide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.179 B 7.397 C 3.61 D 3.30

         Hz     ppm     Int.
    

        739.94   8.262     60
        737.50   8.235    557
        735.44   8.212    184
        730.75   8.160    191
        728.63   8.136    717
        727.19   8.120     61
        726.31   8.110     95
        668.94   7.470     72
        668.44   7.464     49
        666.63   7.444    615
        666.06   7.438    412
        664.44   7.419    179
        659.81   7.368    146
        657.69   7.344    479
        655.81   7.323     49
        655.31   7.317     57
        332.81   3.717    203
        331.00   3.696    248
        326.50   3.646    242
        325.00   3.629    350
        324.19   3.620   1000
        318.69   3.559    495
        317.63   3.547    519
        300.69   3.358    288
        294.44   3.288    360
        292.25   3.264    149
        287.69   3.213    105
        285.94   3.193     92
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder