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MS-IW-0778 ethyl (2-amino-4-thiazolyl)acetate C7H10N2O2S (Mass of molecular ion: 186)
Source Temperature: 190 °C Sample Temperature: 160 °C Reservoir, 75 eV
17.0 1.4 18.0 7.5 27.0 5.0 28.0 2.7 29.0 19.8 31.0 3.4 39.0 1.6 40.0 1.5 41.0 1.8 42.0 3.7 43.0 14.1 44.0 2.7 45.0 14.4 46.0 1.1 55.0 2.0 56.5 3.3 60.0 2.1 67.0 1.7 69.0 9.0 70.0 2.5 71.0 22.1 72.0 8.2 73.0 1.8 81.0 1.4 85.0 1.3 86.0 10.7 87.0 1.9 112.0 1.5 113.0 100.0 114.0 57.0 115.0 8.3 116.0 2.9 127.0 1.2 140.0 4.7 141.0 5.9 186.0 66.9 187.0 7.9 188.0 3.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H10 N2 O2 S 0.039 g : 0.5 ml CDCl3 ethyl (2-amino-4-thiazolyl)acetate Assign. Shift(ppm)
A 6.302 B 5.6 C 4.168 D 3.544 E 1.261
Hz ppm Int.
2518.68 6.303 402 1676.76 4.196 155 1669.56 4.178 462 1662.48 4.160 462 1655.27 4.142 165 1416.75 3.545 680 1416.02 3.544 685 511.11 1.279 519 504.03 1.262 1000 496.83 1.244 512
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