4-溴-3-硝基甲苯

Mass

MS-IW-9453          
4-bromo-3-nitrotoluene
C7H6BrNO2           (Mass of molecular ion:    215)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       2.6
      28.0       3.7
      30.0      10.0
      37.0       2.4
      38.0       4.7
      39.0      18.6
      40.0       2.3
      41.0       1.1
      43.0       1.3
      44.0       1.2
      49.0       1.2
      50.0       8.0
      51.0       9.0
      52.0       3.2
      53.0       2.3
      61.0       3.1
      62.0       9.8
      63.0      30.8
      64.0       8.5
      65.0       5.1
      74.0       3.4
      75.0       3.2
      76.0       1.3
      77.0      17.0
      78.0      42.5
      79.0       3.5
      80.0       2.0
      81.0       1.0
      82.0       1.7
      85.0       1.1
      86.0       2.3
      87.0       2.7
      88.0       2.4
      89.0      59.1
      90.0     100.0
      91.0      11.2
      92.0       1.4
     105.0       2.4
     106.0      11.5
     107.0       1.3
     108.0       1.6
     117.0       2.3
     119.0       2.7
     136.0       3.7
     137.0       1.9
     143.0       2.6
     145.0       2.2
     157.0      13.1
     158.0       1.0
     159.0      12.8
     168.0       1.3
     169.0      28.2
     170.0       3.5
     171.0      27.3
     172.0       2.3
     185.0       5.8
     187.0       5.7
     199.0       1.5
     201.0       1.5
     215.0      49.6
     216.0       4.4
     217.0      48.4
     218.0       4.0

Assign. Shift(ppm) A 7.655 B 7.601 C 7.243 D 2.400

     Hz     ppm     Int.

   3060.79   7.659    163
   3059.33   7.656    171
   3058.84   7.654    165
   3042.11   7.612    213
   3033.94   7.592    240
   2900.02   7.257     98
   2899.29   7.255    107
   2898.56   7.253     88
   2897.95   7.252    107
   2897.22   7.250    105
   2891.85   7.236     89
   2891.11   7.235     97
   2890.38   7.233     79
   2889.65   7.231     95
   2889.04   7.229     92
    959.11   2.400   1000