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网站主页CAS数据库列表 5325-97-3更多图谱1,2,3,4,5,6,7,8-八氢菲(5325-97-3)质谱(MS)

1,2,3,4,5,6,7,8-八氢菲

产品名称 1,2,3,4,5,6,7,8-八氢菲

CAS号5325-97-3

分子式C14H18

分子量186.29

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  • Mass

    MS-NW-0087          
    1,2,3,4,5,6,7,8-octahydrophenanthrene
    C14H18              (Mass of molecular ion:    186)
    

       Source Temperature: 220 °C
       Sample Temperature:  95 °C
       Reservoir, 75 eV
    

          18.0       1.3
          27.0       2.1
          28.0       2.5
          29.0       1.5
          39.0       4.2
          41.0       3.5
          51.0       3.3
          53.0       2.0
          55.0       1.9
          63.0       2.9
          64.0       1.5
          65.0       2.7
          67.0       2.2
          70.5       1.1
          71.0       1.2
          75.0       1.1
          76.0       2.8
          77.0       5.3
          78.0       2.3
          79.0       2.2
          81.0       1.7
          82.0       1.0
          89.0       2.6
          91.0       6.9
          95.0       1.0
          96.0       2.0
          97.0       2.4
         102.0       1.4
         103.0       1.5
         104.0       2.8
         105.0       2.4
         115.0      14.4
         116.0       3.5
         117.0       6.0
         118.0       1.0
         127.0       5.2
         128.0      20.1
         129.0      27.4
         130.0      14.8
         131.0       5.6
         139.0       1.5
         141.0      11.2
         142.0       6.7
         143.0      28.8
         144.0      14.7
         145.0      28.4
         146.0       3.3
         151.0       1.0
         152.0       3.1
         153.0       3.3
         154.0       1.9
         155.0       3.0
         156.0       2.1
         157.0      17.3
         158.0      65.1
         159.0       8.6
         165.0       3.5
         169.0       1.3
         171.0       4.0
         178.0       2.7
         179.0       4.4
         180.0       7.4
         181.0       1.2
         184.0       3.0
         185.0      10.5
         186.0     100.0
         187.0      15.2
         188.0       1.1
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H18 13.0 mg : 0.5 ml CDCl3
    1,2,3,4,5,6,7,8-octahydrophenanthrene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.859 B 2.737 C 2.557 D 1.817 E 1.744

         Hz     ppm     Int.
    

       2741.21   6.860   1000
       1100.22   2.753    217
       1093.99   2.738    398
       1087.77   2.722    205
       1028.56   2.574    197
       1022.34   2.559    443
       1018.92   2.550     54
       1015.87   2.542    253
        739.26   1.850     69
        735.96   1.842     71
        733.28   1.835    144
        729.74   1.826    166
        728.15   1.822    209
        723.39   1.811    177
        721.92   1.807    206
        718.75   1.799     91
        717.90   1.797     82
        717.04   1.795     78
        715.33   1.790    100
        714.11   1.787     77
        712.28   1.783     35
        710.94   1.779     34
        710.21   1.778     40
        708.01   1.772     92
        706.42   1.768    117
        704.59   1.764    136
        703.74   1.761    115
        701.54   1.756    164
        700.20   1.753    235
        698.61   1.749    232
        696.17   1.742    137
        694.34   1.738    222
        692.26   1.733    183
        689.33   1.725    170
        686.28   1.718     63
        683.47   1.711     52
        682.62   1.709     46
    


  • 1H NMR 89.56 MHz
    C14 H18 0.04 ml : 0.5 ml CDCl3
    1,2,3,4,5,6,7,8-octahydrophenanthrene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.84 B 2.73 C 2.55 D 1.82 E 1.73

         Hz     ppm     Int.
    

        612.94   6.844   1000
        250.88   2.802    135
        250.50   2.798    137
        250.00   2.792    136
        249.06   2.781    124
        244.50   2.731    339
        241.69   2.699    215
        240.44   2.685    230
        240.13   2.682    232
        234.75   2.622    165
        234.44   2.618    164
        234.00   2.613    162
        232.88   2.601    173
        231.94   2.590    163
        228.69   2.554    333
        222.69   2.487    194
        218.00   2.435     30
        176.19   1.968     38
        174.56   1.950     64
        173.63   1.939     44
        171.69   1.918     72
        170.81   1.908     69
        168.69   1.884     99
        165.50   1.848    233
        163.69   1.828    244
        162.00   1.809    555
        159.13   1.777    540
        158.50   1.770    536
        155.50   1.737    460
        153.31   1.712    220
        151.63   1.694    185
        149.38   1.668     89
        147.19   1.644     42
        146.88   1.641     42
        146.56   1.637     44
        145.50   1.625     52
        145.13   1.621     51
        144.31   1.612     36
        144.00   1.608     36
        143.63   1.604     39
    

in CDCl3



liquid film



4880 A,200 M,liquid