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MassMS-NW-4805 alpha-hydroxyphenylacetonitrile C8H7NO (Mass of molecular ion: 133)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 1.5 26.0 5.5 27.0 38.3 28.0 1.8 29.0 3.1 37.0 3.3 38.0 3.9 39.0 7.6 49.0 2.1 50.0 17.3 51.0 38.1 52.0 10.8 53.0 1.2 54.0 1.4 61.0 1.3 62.0 1.9 63.0 3.4 73.0 1.6 74.0 5.8 75.0 3.1 76.0 4.5 77.0 94.1 78.0 20.2 79.0 9.4 89.0 2.7 104.0 3.7 105.0 100.0 106.0 88.7 107.0 8.5 115.0 8.9 116.0 7.0 132.0 11.2 133.0 17.3 134.0 1.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H7 N O 0.04 ml : 0.5 ml CDCl3 alpha-hydroxyphenylacetonitrile 
Assign. Shift(ppm)
A 7.70 to 7.22 B 5.460 C 3.75
Hz ppm Int.678.63 7.578 34 676.19 7.551 32 674.44 7.531 54 673.06 7.516 59 672.56 7.510 57 671.50 7.498 49 670.19 7.484 67 669.50 7.476 69 669.00 7.470 69 668.50 7.465 88 666.94 7.447 317 666.00 7.437 904 664.44 7.419 1000 662.13 7.394 297 660.69 7.378 127 659.94 7.369 104 658.69 7.355 49 657.06 7.337 103 655.81 7.323 32 489.06 5.461 168 336.06 3.753 76
in CDCl3
CCl4 solution
liquid film
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