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MS-NW-6151 5,6,7,8-tetrahydro-1-naphthol C10H12O (Mass of molecular ion: 148)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 3.8 38.0 1.4 39.0 8.8 40.0 1.2 41.0 3.9 43.0 1.0 50.0 2.7 51.0 8.3 52.0 2.6 53.0 3.2 55.0 2.7 57.5 1.4 58.0 1.3 62.0 1.7 63.0 5.1 63.5 1.1 64.0 3.4 65.0 6.3 65.5 2.0 66.0 3.4 66.5 1.0 72.0 2.1 72.5 1.1 73.0 3.3 74.0 2.5 75.0 1.3 76.0 1.0 77.0 9.0 78.0 2.9 79.0 3.4 89.0 2.3 90.0 1.0 91.0 21.4 92.0 8.1 93.0 1.1 94.0 1.3 102.0 1.4 103.0 3.4 104.0 1.8 105.0 4.1 107.0 24.2 108.0 2.1 115.0 8.0 116.0 2.1 117.0 2.8 119.0 5.7 120.0 99.6 121.0 9.2 127.0 3.7 128.0 4.3 129.0 4.5 130.0 2.9 131.0 10.8 132.0 4.9 133.0 13.2 134.0 1.4 144.0 1.1 145.0 2.6 146.0 1.7 147.0 24.0 148.0 100.0 149.0 11.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H12 O 0.049 g : 0.5 ml CDCl3 5,6,7,8-tetrahydro-1-naphthol Assign. Shift(ppm)
A 6.964 B 6.673 C 6.576 D 4.87 E 2.736 F 2.613 G *1 1.81 J *1 1.75
Hz ppm Int.
2791.63 6.986 182 2783.94 6.966 384 2776.00 6.947 227 2670.17 6.682 286 2663.33 6.665 247 2662.84 6.663 251 2632.20 6.587 307 2631.71 6.586 307 2624.27 6.567 279 2623.78 6.566 278 1948.00 4.875 1000 1099.98 2.753 247 1093.75 2.737 446 1087.65 2.722 252 1050.90 2.630 236 1044.68 2.614 499 1038.21 2.598 285 736.82 1.844 72 733.52 1.836 77 731.08 1.830 153 730.10 1.827 139 727.42 1.821 202 726.93 1.819 201 725.34 1.815 217 723.14 1.810 119 721.19 1.805 198 719.48 1.801 249 717.90 1.797 211 715.70 1.791 111 714.48 1.788 108 713.26 1.785 144 712.40 1.783 132 710.69 1.779 127 709.59 1.776 151 707.64 1.771 145 704.96 1.764 217 703.13 1.760 255 701.66 1.756 259 697.51 1.746 257 695.43 1.741 246 692.50 1.733 184 689.33 1.725 91 686.52 1.718 72 685.67 1.716 62
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