-
MassMS-NW-7392 1,2,3,4-tetrahydro-1-naphthol C10H12O (Mass of molecular ion: 148)
Source Temperature: 210 °C Sample Temperature: 190 °C Reservoir, 75 eV
17.0 1.1 18.0 5.2 27.0 1.8 28.0 1.0 38.0 1.2 39.0 5.2 41.0 1.1 50.0 4.7 51.0 11.4 52.0 2.2 61.0 1.0 62.0 2.3 63.0 8.9 63.5 3.4 64.0 11.8 64.5 2.9 65.0 5.8 74.0 3.6 75.0 3.4 76.0 2.9 77.0 7.7 78.0 3.9 87.0 1.1 89.0 3.5 90.0 2.1 91.0 8.9 92.0 1.8 98.0 1.0 101.0 2.3 102.0 5.4 103.0 2.3 104.0 2.4 105.0 3.8 115.0 40.9 116.0 5.0 117.0 1.4 118.0 2.6 119.0 6.0 120.0 10.7 121.0 1.1 126.0 4.2 127.0 17.6 128.0 40.0 129.0 77.7 130.0 100.0 131.0 11.7 132.0 1.2 146.0 1.9 147.0 4.9 148.0 5.0
90 MHz in CDCl3
400 MHz in CDCl3
-
1H NMR 89.56 MHz C10 H12 O 0.04 ml : 0.5 ml CDCl3 1,2,3,4-tetrahydro-1-naphthol 
Assign. Shift(ppm)
A 7.38 B 7.28 to 6.96 C 4.72 D 2.74 E 2.02 F 2.14 to 1.47
Hz ppm Int.666.94 7.447 128 665.38 7.430 76 664.75 7.423 107 663.94 7.414 117 662.56 7.398 194 661.88 7.391 269 660.19 7.372 88 658.19 7.350 316 654.75 7.311 134 650.81 7.267 69 649.81 7.256 89 647.13 7.226 530 643.19 7.182 523 641.50 7.163 782 640.44 7.151 266 639.25 7.138 380 638.00 7.124 1000 636.63 7.109 532 635.88 7.101 515 634.94 7.090 372 633.88 7.078 183 632.38 7.061 195 631.81 7.055 172 631.25 7.049 163 629.94 7.034 89 628.63 7.020 59 627.13 7.003 64 626.25 6.993 73 427.19 4.770 146 426.56 4.763 143 425.81 4.755 127 423.19 4.726 245 422.81 4.721 244 419.19 4.681 146 253.81 2.834 88 253.38 2.830 93 251.06 2.804 219 249.31 2.784 162 246.75 2.756 352 244.88 2.735 362 240.75 2.689 228 240.31 2.684 223 236.63 2.643 65 186.00 2.077 95 184.81 2.064 123 180.56 2.017 681 177.56 1.983 281 175.75 1.963 375 174.81 1.952 448 173.69 1.940 391 172.81 1.930 335 171.75 1.918 478 170.06 1.899 587 169.50 1.893 628 168.75 1.885 669 166.19 1.856 462 164.88 1.842 378 163.94 1.831 398 163.56 1.827 398 159.25 1.779 134 158.94 1.775 137 158.19 1.767 144 155.94 1.742 107 155.19 1.733 119 153.56 1.715 92 152.81 1.707 123 152.19 1.700 104 151.56 1.693 120
-
1H NMR 399.65 MHz C10 H12 O 0.020 g : 0.5 ml CDCl3 1,2,3,4-tetrahydro-1-naphthol Assign. Shift(ppm)
A 7.419 B 7.21 to 7.18 C 7.099 D 4.765 E *1 2.81 F *1 2.72 G 2.05 to 1.92 J *2 1.89 K 1.84 L *2 1.77
Hz ppm Int.2970.09 7.432 278 2966.67 7.424 295 2965.58 7.421 299 2963.87 7.417 187 2963.13 7.415 171 2960.94 7.409 351 2884.89 7.219 87 2883.67 7.216 68 2880.25 7.207 933 2877.56 7.201 441 2876.34 7.198 522 2875.12 7.195 438 2873.90 7.192 564 2871.09 7.185 1000 2869.02 7.179 83 2868.41 7.178 78 2867.80 7.176 84 2866.58 7.173 130 2840.94 7.109 325 2838.75 7.104 158 2838.13 7.102 162 2836.55 7.098 267 2835.45 7.095 231 2832.15 7.087 205 1904.91 4.767 235 1135.99 2.843 102 1130.62 2.830 70 1124.76 2.815 147 1119.14 2.801 247 1114.26 2.789 165 1100.59 2.754 107 1094.60 2.739 150 1093.02 2.735 191 1089.84 2.727 67 1087.40 2.721 129 1086.91 2.720 128 1084.96 2.715 64 1078.25 2.698 79 1077.27 2.696 87 1076.66 2.695 89 1076.05 2.693 88 801.51 2.006 109 800.90 2.005 93 798.95 2.000 159 798.22 1.998 170 797.00 1.995 248 795.41 1.991 121 794.31 1.988 210 791.63 1.981 337 790.28 1.978 175 789.55 1.976 204 786.87 1.969 468 783.57 1.961 172 781.98 1.957 198 780.88 1.954 220 779.30 1.950 146 778.20 1.948 167 777.34 1.946 118 776.86 1.944 131 776.00 1.942 157 773.44 1.936 166 771.85 1.932 138 770.63 1.929 105 769.53 1.926 141 768.19 1.923 174 766.24 1.918 103 764.53 1.913 95 763.18 1.910 152 762.33 1.908 199 761.11 1.905 186 757.93 1.897 117 756.96 1.895 78 755.37 1.891 179 754.88 1.889 167 753.05 1.885 124 752.20 1.883 101 751.10 1.880 160 750.49 1.878 151 745.36 1.866 101 744.75 1.864 89 733.15 1.835 341 725.10 1.815 77 724.12 1.812 94 720.95 1.804 122 714.60 1.789 186 711.43 1.781 194 709.35 1.775 118 708.25 1.773 175 705.69 1.766 150 704.22 1.763 106 702.39 1.758 85 700.68 1.754 67 699.71 1.751 89 698.36 1.748 110 697.63 1.746 101 697.27 1.745 108 692.38 1.733 65
in CDCl3
liquid film
更多供应商
