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MassMS-NW-8766 o-iodoanisole C7H7IO (Mass of molecular ion: 234)
Source Temperature: 270 °C Sample Temperature: 130 °C Reservoir, 75 eV
38.0 2.7 39.0 1.3 50.0 4.4 51.0 5.5 62.0 1.8 63.0 8.0 64.0 10.5 74.0 1.6 75.0 1.2 76.0 5.0 77.0 16.6 78.0 2.0 79.0 2.4 92.0 29.7 93.0 2.0 117.0 1.2 127.0 1.3 191.0 7.7 203.0 1.4 219.0 24.5 220.0 1.8 234.0 100.0 235.0 7.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H7 I O 0.05 ml : 0.5 ml CDCl3 o-iodoanisole 
Assign. Shift(ppm)
A 7.734 B 7.257 C 6.766 D 6.668 E 3.804 J(A,B)=1.6HZ J(A,D)=7.6HZ J(B,C)=8.3HZ J(B,D)=7.4HZ J(C,D)=1.3HZ
Hz ppm Int.3095.83 7.747 150 3094.12 7.743 163 3088.01 7.727 163 3086.43 7.723 171 2909.18 7.280 84 2907.59 7.276 83 2901.73 7.261 100 2900.88 7.259 122 2900.15 7.257 129 2899.29 7.255 122 2893.55 7.241 100 2891.97 7.237 99 2708.74 6.778 126 2707.40 6.775 148 2700.44 6.758 121 2699.10 6.754 138 2673.22 6.689 104 2671.88 6.686 104 2665.53 6.670 147 2664.06 6.666 149 2658.08 6.652 99 2656.74 6.648 98 1520.39 3.805 1000
in CDCl3
liquid film
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