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网站主页CAS数据库列表 5283-66-9更多图谱辛基三氯硅烷(5283-66-9)Raman光谱

辛基三氯硅烷

产品名称 辛基三氯硅烷

CAS号5283-66-9

分子式C8H17Cl3Si

分子量247.66

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  • Mass

    MS-NW-3330          
    trichlorooctylsilane
    C8H17Cl3Si          (Mass of molecular ion:    246)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          27.0       8.8
          28.0       2.1
          29.0      14.7
          39.0       6.8
          40.0       1.3
          41.0      24.9
          42.0      11.8
          43.0     100.0
          44.0       3.2
          53.0       1.5
          54.0       1.3
          55.0      13.4
          56.0      12.4
          57.0      48.7
          58.0       2.4
          63.0       2.0
          65.0       1.0
          69.0       4.1
          70.0       4.3
          71.0      25.9
          72.0       1.6
          84.0       2.1
          85.0      40.4
          86.0       2.9
          98.0       1.4
          99.0       1.7
         100.0       1.1
         101.0       1.1
         117.0       1.1
         125.0       1.5
         127.0       1.1
         133.0      14.9
         135.0      15.0
         137.0       5.0
         139.0       2.9
         141.0       2.2
         153.0       2.8
         155.0       1.8
         161.0       5.3
         163.0       5.0
         165.0       1.7
         167.0       2.2
         169.0       1.3
         174.0       1.7
         175.0      13.0
         176.0       3.0
         177.0      13.4
         178.0       1.8
         179.0       4.8
         189.0       4.6
         190.0       1.1
         191.0       4.1
         193.0       1.4
         203.0       3.7
         204.0       1.0
         205.0       3.4
         207.0       1.3
         217.0       2.2
         219.0       2.3
         246.0       1.2
         248.0       1.2
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H17 Cl3 Si 0.04 ml : 0.5 ml CDCl3
    trichlorooctylsilane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.76 to 1.08 B 0.89

         Hz     ppm     Int.
    

        154.25   1.723     36
        153.94   1.719     39
        153.31   1.712     39
        152.56   1.704     39
        152.19   1.700     41
        151.88   1.696     43
        151.25   1.689     43
        150.56   1.682     47
        148.75   1.661     62
        148.44   1.658     62
        147.88   1.652     63
        147.56   1.648     61
        146.25   1.633     70
        145.88   1.629     70
        145.38   1.624     73
        144.50   1.614     77
        143.44   1.602     85
        141.25   1.578    113
        134.94   1.507    252
        129.63   1.448    496
        127.06   1.419    372
        126.75   1.416    368
        125.63   1.403    367
        115.88   1.294    997
        115.19   1.287   1000
        104.19   1.164     39
        103.00   1.151     37
        102.44   1.144     36
        102.06   1.140     36
         84.63   0.945    167
         79.31   0.886    549
         73.25   0.818    114
    


  • 1H NMR 399.65 MHz
    C8 H17 Cl3 Si 0.05 ml : 0.5 ml CDCl3
    trichlorooctylsilane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.58 B 1.48 to 1.360 C 1.36 to 1.210 D 0.89

         Hz     ppm     Int.
    

        648.68   1.624     51
        647.09   1.620     50
        643.31   1.610     61
        641.60   1.606    127
        639.04   1.599    104
        636.96   1.594     95
        634.89   1.589    136
        633.30   1.585    191
        632.45   1.583    180
        630.00   1.577    101
        628.66   1.574    110
        627.32   1.570    136
        625.37   1.565    199
        622.19   1.557    121
        620.48   1.553     61
        617.68   1.546    105
        616.46   1.543    100
        584.72   1.464     31
        576.54   1.443     78
        576.05   1.442     79
        574.71   1.439     82
        569.21   1.425    179
        564.94   1.414    606
        562.01   1.407    271
        559.69   1.401    333
        556.88   1.394    348
        555.79   1.391    380
        548.83   1.374    288
        548.22   1.372    292
        544.19   1.362     64
        543.58   1.361     64
        530.52   1.328    215
        523.68   1.311    381
        518.68   1.298    545
        517.21   1.295    569
        515.14   1.289    655
        512.94   1.284    728
        365.72   0.916     60
        361.33   0.905    342
        354.61   0.888   1000
        347.53   0.870    379
    

liquid film