图谱信息 供应商 相关产品
网站主页CAS数据库列表 52727-57-8更多图谱5-溴氨基苯甲酸甲酯(52727-57-8)质谱(MS)

5-溴氨基苯甲酸甲酯

产品名称 5-溴氨基苯甲酸甲酯

CAS号52727-57-8

分子式C8H8BrNO2

分子量230.06

展开


  • Mass

    MS-KW-0271          
    methyl 5-bromoanthranilate
    C8H8BrNO2           (Mass of molecular ion:    229)
    

       Source Temperature: 240 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       3.9
          28.0       3.3
          29.0       2.0
          31.0       1.7
          37.0       2.7
          38.0       5.2
          39.0       5.5
          40.0       1.9
          41.0       5.7
          44.0       1.7
          44.5       2.5
          45.0       1.5
          45.5       9.4
          50.0       2.3
          51.0       2.6
          52.0      13.0
          53.0       2.4
          59.0       1.4
          61.0       3.7
          62.0       8.9
          63.0      28.1
          64.0      11.5
          65.0       6.9
          66.0       1.2
          74.0       2.2
          75.0       2.8
          77.0       1.4
          78.0       1.6
          79.0       1.7
          80.0       1.3
          82.0       1.2
          85.0       3.8
          86.0       3.8
          88.0       1.7
          89.0       3.8
          90.0      27.6
          91.0      20.9
          92.0       3.4
          99.0       2.5
         100.0       2.5
         107.0       2.1
         114.0       2.6
         115.0       2.6
         117.0       2.5
         118.0       1.2
         119.0       1.7
         135.0       3.1
         142.0       2.1
         143.0       7.8
         144.0       2.5
         145.0       7.3
         168.0       1.7
         169.0      21.3
         170.0      29.2
         171.0      23.3
         172.0      26.9
         173.0       2.8
         197.0     100.0
         198.0      26.0
         199.0      98.9
         200.0      25.5
         201.0       2.1
         229.0      80.5
         230.0       8.1
         231.0      79.3
         232.0       7.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8H8BrNO2 0.039 g : 0.5 ml CDCl3
    methyl 5-bromoanthranilate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.955 B 7.311 C 6.547 D 5.7 E 3.861

         Hz     ppm     Int.
    

       3181.52   7.959    165
       3179.08   7.953    167
       2928.35   7.325     92
       2925.91   7.319     88
       2919.56   7.303     96
       2917.12   7.297     92
       2621.83   6.559    156
       2613.04   6.537    149
       2280.64   5.705      8
       1616.34   4.044      6
       1543.71   3.862   1000
       1469.12   3.675      5
    

in CDCl3



KBr disk



Nujol